2-Diazo-N-(4-methoxy-phenyl)-N-[2-(3-nitro-phenyl)-ethyl]-malonamic acid (1S,2R,3R,4S)-4,7,7-trimethyl-3-naphthalen-1-yl-bicyclo[2.2.1]hept-2-yl ester

Base Information

Chemical Name:2-Diazo-N-(4-methoxy-phenyl)-N-[2-(3-nitro-phenyl)-ethyl]-malonamic acid (1S,2R,3R,4S)-4,7,7-trimethyl-3-naphthalen-1-yl-bicyclo[2.2.1]hept-2-yl ester
CAS No.:174618-61-2
Molecular Formula:C₃₈H₃₈N₄O₆
Molecular Weight:646.743
Hs Code.:

2-Diazo-N-(4-methoxy-phenyl)-N-[2-(3-nitro-phenyl)-ethyl]-malonamic acid (1S,2R,3R,4S)-4,7,7-trimethyl-3-naphthalen-1-yl-bicyclo[2.2.1]hept-2-yl ester

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Chemical Property of 2-Diazo-N-(4-methoxy-phenyl)-N-[2-(3-nitro-phenyl)-ethyl]-malonamic acid (1S,2R,3R,4S)-4,7,7-trimethyl-3-naphthalen-1-yl-bicyclo[2.2.1]hept-2-yl ester

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Technology Process of 2-Diazo-N-(4-methoxy-phenyl)-N-[2-(3-nitro-phenyl)-ethyl]-malonamic acid (1S,2R,3R,4S)-4,7,7-trimethyl-3-naphthalen-1-yl-bicyclo[2.2.1]hept-2-yl ester

There total 3 articles about 2-Diazo-N-(4-methoxy-phenyl)-N-[2-(3-nitro-phenyl)-ethyl]-malonamic acid (1S,2R,3R,4S)-4,7,7-trimethyl-3-naphthalen-1-yl-bicyclo[2.2.1]hept-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 210585-36-7
N-(4-Methoxy-phenyl)-N-[2-(3-nitro-phenyl)-ethyl]-malonamic acid (1S,2R,3R,4S)-4,7,7-trimethyl-3-naphthalen-1-yl-bicyclo[2.2.1]hept-2-yl ester

: 174618-61-2
2-Diazo-N-(4-methoxy-phenyl)-N-[2-(3-nitro-phenyl)-ethyl]-malonamic acid (1S,2R,3R,4S)-4,7,7-trimethyl-3-naphthalen-1-yl-bicyclo[2.2.1]hept-2-yl ester

Guidance literature:: With potassium hydride; Methanesulfonyl azide; In tetrahydrofuran;
DOI:10.1016/0040-4039(95)02115-9

Reference yield:

: (4-Methoxy-phenyl)-[2-(3-nitro-phenyl)-ethyl]-amine

: 174618-61-2
2-Diazo-N-(4-methoxy-phenyl)-N-[2-(3-nitro-phenyl)-ethyl]-malonamic acid (1S,2R,3R,4S)-4,7,7-trimethyl-3-naphthalen-1-yl-bicyclo[2.2.1]hept-2-yl ester

Guidance literature:: Multi-step reaction with 3 steps

3: MsN₃, KH / tetrahydrofuran

With potassium hydride; Methanesulfonyl azide; In tetrahydrofuran;
DOI:10.1016/0040-4039(95)02115-9

Reference yield:

: 210585-27-6
N-(4-Methoxy-phenyl)-N-[2-(3-nitro-phenyl)-ethyl]-malonamic acid

: 174618-61-2
2-Diazo-N-(4-methoxy-phenyl)-N-[2-(3-nitro-phenyl)-ethyl]-malonamic acid (1S,2R,3R,4S)-4,7,7-trimethyl-3-naphthalen-1-yl-bicyclo[2.2.1]hept-2-yl ester

Guidance literature:: Multi-step reaction with 2 steps

2: MsN₃, KH / tetrahydrofuran

With potassium hydride; Methanesulfonyl azide; In tetrahydrofuran;
DOI:10.1016/0040-4039(95)02115-9