2-azido-4,6-O-benzylidene-2-deoxy-3-O-trifluoromethylsulfonyl-α-D-altropyranosyl 2-azido-4,6-O-benzylidene-2-deoxy-3-O-trifluoromethylsulfonyl-α-D-altropyranoside

Base Information

Chemical Name:2-azido-4,6-O-benzylidene-2-deoxy-3-O-trifluoromethylsulfonyl-α-D-altropyranosyl 2-azido-4,6-O-benzylidene-2-deoxy-3-O-trifluoromethylsulfonyl-α-D-altropyranoside
CAS No.:103954-88-7
Molecular Formula:C₂₈H₂₆F₆N₆O₁₃S₂
Molecular Weight:832.669
Hs Code.:

2-azido-4,6-O-benzylidene-2-deoxy-3-O-trifluoromethylsulfonyl-α-D-altropyranosyl 2-azido-4,6-O-benzylidene-2-deoxy-3-O-trifluoromethylsulfonyl-α-D-altropyranoside

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Chemical Property of 2-azido-4,6-O-benzylidene-2-deoxy-3-O-trifluoromethylsulfonyl-α-D-altropyranosyl 2-azido-4,6-O-benzylidene-2-deoxy-3-O-trifluoromethylsulfonyl-α-D-altropyranoside

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Technology Process of 2-azido-4,6-O-benzylidene-2-deoxy-3-O-trifluoromethylsulfonyl-α-D-altropyranosyl 2-azido-4,6-O-benzylidene-2-deoxy-3-O-trifluoromethylsulfonyl-α-D-altropyranoside

There total 1 articles about 2-azido-4,6-O-benzylidene-2-deoxy-3-O-trifluoromethylsulfonyl-α-D-altropyranosyl 2-azido-4,6-O-benzylidene-2-deoxy-3-O-trifluoromethylsulfonyl-α-D-altropyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 40094-07-3
2-azido-4,6-O-benzylidene-2-deoxy-α-D-altropyranosyl 2-azido-4,6-O-benzylidene-2-deoxy-α-D-altropyranoside

: 358-23-6
trifluoromethylsulfonic anhydride

: 103954-88-7
2-azido-4,6-O-benzylidene-2-deoxy-3-O-trifluoromethylsulfonyl-α-D-altropyranosyl 2-azido-4,6-O-benzylidene-2-deoxy-3-O-trifluoromethylsulfonyl-α-D-altropyranoside

Guidance literature:: In pyridine; dichloromethane; 1.) 15 min, 0 deg C, 2.) 30 min, room temp.;
DOI:10.1016/0008-6215(86)85025-X

Reference yield: 73.7%

: 103954-88-7
2-azido-4,6-O-benzylidene-2-deoxy-3-O-trifluoromethylsulfonyl-α-D-altropyranosyl 2-azido-4,6-O-benzylidene-2-deoxy-3-O-trifluoromethylsulfonyl-α-D-altropyranoside

: 2,3-diazido-4,6-O-benzylidene-2,3-dideoxy-α-D-mannopyranosyl 2-azido-4,6-O-benzylidene-2,3-dideoxy-α-D-threo-hex-3-enopyranoside

: 103954-78-5
2,3-diazido-4,6-O-benzylidene-2,3-dideoxy-α-D-mannopyranosyl 2,3-diazido-4,6-O-benzylidene-2,3-dideoxy-α-D-mannopyranoside

: 2,3-diazido-4,6-O-benzylidene-2,3-dideoxy-α-D-mannopyranosyl 2-azido-4,6-O-benzylidene-2-deoxy-α-D-altropyranoside

Guidance literature:: With tetramethylguanidinum azide; In dichloromethane; benzene; 1.) 18 h, room temp., 2.) 2 h, reflux;
DOI:10.1016/0008-6215(86)85025-X

Reference yield:

: 103954-88-7
2-azido-4,6-O-benzylidene-2-deoxy-3-O-trifluoromethylsulfonyl-α-D-altropyranosyl 2-azido-4,6-O-benzylidene-2-deoxy-3-O-trifluoromethylsulfonyl-α-D-altropyranoside

: Acetic acid (4aR,6R,7S,8S,8aS)-7-azido-6-((4aR,6R,7S,8R,8aS)-7,8-diazido-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.2 percent / tetramethylguanidinium azide / CH₂Cl₂; benzene / 1.) 18 h, room temp., 2.) 2 h, reflux

2: pyridine

With tetramethylguanidinum azide; In pyridine; dichloromethane; benzene;
DOI:10.1016/0008-6215(86)85025-X