-2-(1-Diphenylphosphinoylethyl)cyclohexanone

Base Information

Chemical Name:-2-(1-Diphenylphosphinoylethyl)cyclohexanone
CAS No.:108791-03-3
Molecular Formula:C₂₀H₂₃O₂P
Molecular Weight:326.375
Hs Code.:

<R-(R*,S*)>-2-(1-Diphenylphosphinoylethyl)cyclohexanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of -2-(1-Diphenylphosphinoylethyl)cyclohexanone

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Technology Process of -2-(1-Diphenylphosphinoylethyl)cyclohexanone

There total 8 articles about -2-(1-Diphenylphosphinoylethyl)cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.5%

: 144863-57-0,144939-50-4
-2-(1-Diphenylphosphinoylethyl)cyclohexanol

: 108791-03-3,108791-05-5,144863-60-5,144939-51-5,144939-52-6
-2-(1-Diphenylphosphinoylethyl)cyclohexanone

Guidance literature:: With sodium hypochlorite; acetic acid;
DOI:10.1039/P19920002155

Reference yield: 87.0%

: 144863-57-0,144939-50-4
-2-(1-Diphenylphosphinoylethyl)cyclohexanol

: 108791-03-3,108791-05-5,144863-60-5,144939-51-5,144939-52-6
-2-(1-Diphenylphosphinoylethyl)cyclohexanone

Guidance literature:: With sodium hypochlorite; acetic acid; for 168h; Ambient temperature;
DOI:10.1039/P19920002155

Reference yield:

: 1733-57-9
ethydiphenylphosphine oxide

: 108791-03-3,108791-05-5,144863-60-5,144939-51-5,144939-52-6
-2-(1-Diphenylphosphinoylethyl)cyclohexanone

Guidance literature:: Multi-step reaction with 2 steps

1: 1) BuLi / 1) hexane, THF, 0 deg C, 2) a) -70 deg C to r.t., b) 14 h, r.t.

2: 89.5 percent / aq. NaOCl, gl. AcOH

With sodium hypochlorite; n-butyllithium; acetic acid;
DOI:10.1039/P19920002155