Ethanone, 1-(4-methylphenyl)-2-(5-methyl-1,3,4-thiadiazol-2-yl)-

Base Information

Chemical Name:Ethanone, 1-(4-methylphenyl)-2-(5-methyl-1,3,4-thiadiazol-2-yl)-
CAS No.:125488-07-5
Molecular Formula:C12H12N2OS
Molecular Weight:232.30100
Hs Code.:
Mol file:125488-07-5.mol

Synonyms:2-(5-Methyl-[1,3,4]thiadiazol-2-yl)-1-p-tolyl-ethanone;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethanone, 1-(4-methylphenyl)-2-(5-methyl-1,3,4-thiadiazol-2-yl)-

Chemical Property:

PSA：71.09000
LogP:2.58030

Purity/Quality:

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Technology Process of Ethanone, 1-(4-methylphenyl)-2-(5-methyl-1,3,4-thiadiazol-2-yl)-

There total 3 articles about Ethanone, 1-(4-methylphenyl)-2-(5-methyl-1,3,4-thiadiazol-2-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 4-methyl-benzoic acid 2-(5-methyl-[1,3,4]thiadiazol-2-yl)-1-p-tolyl-vinyl ester

: 125488-07-5
1-(4-Methylphenyl)-2-[5-methyl-1,3,4-thiadiazol-2-yl]ethanon

Guidance literature:: With hydrogenchloride; In isopropyl alcohol; for 8h; Heating;
DOI:10.1515/znb-2004-0403

Reference yield:

: 27464-82-0
2,5-dimethyl-1,3,4-thiadiazole

: 94-08-6
4-methylbenzoic acid ethyl ester

: 125488-07-5
1-(4-Methylphenyl)-2-[5-methyl-1,3,4-thiadiazol-2-yl]ethanon

Guidance literature:: 2,5-dimethyl-1,3,4-thiadiazole; With sodium hydride; In toluene; at 30 - 60 ℃; for 1h;

4-methylbenzoic acid ethyl ester; In toluene; for 4h; Heating;
DOI:10.1515/znb-2004-0403

Reference yield:

: 874-60-2
4-methyl-benzoyl chloride

: 125488-07-5
1-(4-Methylphenyl)-2-[5-methyl-1,3,4-thiadiazol-2-yl]ethanon

Guidance literature:: Multi-step reaction with 2 steps

1: 34 percent / Et₃N / CH₂Cl₂ / 4 h / Heating

2: 69 percent / aq. HCl / propan-2-ol / 8 h / Heating

With hydrogenchloride; triethylamine; In dichloromethane; isopropyl alcohol;
DOI:10.1515/znb-2004-0403