Technology Process of C15H23F2NO6
There total 6 articles about C15H23F2NO6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dmap / tetrahydrofuran / 5.25 h / 20 °C
2: 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide / water; 1,4-dioxane / 30 °C
3: 2,6-dimethylpyridine; diethylamino-sulfur trifluoride / dichloromethane / 12 h / 10 - 20 °C
4: sodium hydroxide / 20 °C
With
2,6-dimethylpyridine; dmap; sodium periodate; osmium(VIII) oxide; diethylamino-sulfur trifluoride; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1021/acs.oprd.9b00469
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dmap / tetrahydrofuran / 5.25 h / 20 °C
2: 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide / water; 1,4-dioxane / 30 °C
3: 2,6-dimethylpyridine; diethylamino-sulfur trifluoride / dichloromethane / 12 h / 10 - 20 °C
4: sodium hydroxide / 20 °C
With
2,6-dimethylpyridine; dmap; sodium periodate; osmium(VIII) oxide; diethylamino-sulfur trifluoride; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1021/acs.oprd.9b00469
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium dihydrogenphosphate / n-heptane; dichloromethane; water
2: 2,6-dimethylpyridine; diethylamino-sulfur trifluoride / dichloromethane / 12 h / 10 - 20 °C
3: sodium hydroxide / 20 °C
With
2,6-dimethylpyridine; potassium dihydrogenphosphate; diethylamino-sulfur trifluoride; sodium hydroxide;
In
n-heptane; dichloromethane; water;
DOI:10.1021/acs.oprd.9b00469