N,N-Dioctadecyl-phthalamic acid (2R,3S,4S,5R,6S)-3,4,5-tris-(2-tert-butoxycarbonylamino-acetoxy)-6-methoxy-tetrahydro-pyran-2-ylmethyl ester

Base Information

Chemical Name:N,N-Dioctadecyl-phthalamic acid (2R,3S,4S,5R,6S)-3,4,5-tris-(2-tert-butoxycarbonylamino-acetoxy)-6-methoxy-tetrahydro-pyran-2-ylmethyl ester
CAS No.:290300-59-3
Molecular Formula:C₇₂H₁₂₄N₄O₁₇
Molecular Weight:1317.79
Hs Code.:

N,N-Dioctadecyl-phthalamic acid (2R,3S,4S,5R,6S)-3,4,5-tris-(2-tert-butoxycarbonylamino-acetoxy)-6-methoxy-tetrahydro-pyran-2-ylmethyl ester

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Chemical Property of N,N-Dioctadecyl-phthalamic acid (2R,3S,4S,5R,6S)-3,4,5-tris-(2-tert-butoxycarbonylamino-acetoxy)-6-methoxy-tetrahydro-pyran-2-ylmethyl ester

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Technology Process of N,N-Dioctadecyl-phthalamic acid (2R,3S,4S,5R,6S)-3,4,5-tris-(2-tert-butoxycarbonylamino-acetoxy)-6-methoxy-tetrahydro-pyran-2-ylmethyl ester

There total 5 articles about N,N-Dioctadecyl-phthalamic acid (2R,3S,4S,5R,6S)-3,4,5-tris-(2-tert-butoxycarbonylamino-acetoxy)-6-methoxy-tetrahydro-pyran-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35526-05-7
6-O-benzyl-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

: 290300-59-3
N,N-Dioctadecyl-phthalamic acid (2R,3S,4S,5R,6S)-3,4,5-tris-(2-tert-butoxycarbonylamino-acetoxy)-6-methoxy-tetrahydro-pyran-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: HCl

2: BOP; Et₃N / CH₂Cl₂

3: H₂ / Pd/C / ethanol

4: pyridine; DMAP

5: BOP; Et₃N / CH₂Cl₂

With pyridine; hydrogenchloride; dmap; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; 1: Methanolysis / 2: Acylation / 3: Hydrogenolysis / 4: Acylation / 5: Acylation;
DOI:10.1016/S0960-894X(00)00251-1

Reference yield:

: 23392-30-5
methyl 6-O-benzyl-α-D-galactopyranoside

: 290300-59-3
N,N-Dioctadecyl-phthalamic acid (2R,3S,4S,5R,6S)-3,4,5-tris-(2-tert-butoxycarbonylamino-acetoxy)-6-methoxy-tetrahydro-pyran-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: BOP; Et₃N / CH₂Cl₂

2: H₂ / Pd/C / ethanol

3: pyridine; DMAP

4: BOP; Et₃N / CH₂Cl₂

With pyridine; dmap; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; 1: Acylation / 2: Hydrogenolysis / 3: Acylation / 4: Acylation;
DOI:10.1016/S0960-894X(00)00251-1

Reference yield:

: 290300-51-5
tert-Butoxycarbonylamino-acetic acid (2R,3S,4S,5R,6S)-2-benzyloxymethyl-3,5-bis-(2-tert-butoxycarbonylamino-acetoxy)-6-methoxy-tetrahydro-pyran-4-yl ester

: 290300-59-3
N,N-Dioctadecyl-phthalamic acid (2R,3S,4S,5R,6S)-3,4,5-tris-(2-tert-butoxycarbonylamino-acetoxy)-6-methoxy-tetrahydro-pyran-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd/C / ethanol

2: pyridine; DMAP

3: BOP; Et₃N / CH₂Cl₂

With pyridine; dmap; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; 1: Hydrogenolysis / 2: Acylation / 3: Acylation;
DOI:10.1016/S0960-894X(00)00251-1