(μ,η2-3,4-bis(4'-methoxyphenyl)-1,5-hexadiyne)bis(dicobalt hexacarbonyl)

Base Information

Chemical Name:(μ,η2-3,4-bis(4'-methoxyphenyl)-1,5-hexadiyne)bis(dicobalt hexacarbonyl)
CAS No.:610802-79-4
Molecular Formula:C₃₂H₁₈Co₄O₁₄
Molecular Weight:862.459
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (μ,η2-3,4-bis(4'-methoxyphenyl)-1,5-hexadiyne)bis(dicobalt hexacarbonyl)

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Technology Process of (μ,η2-3,4-bis(4'-methoxyphenyl)-1,5-hexadiyne)bis(dicobalt hexacarbonyl)

There total 1 articles about (μ,η2-3,4-bis(4'-methoxyphenyl)-1,5-hexadiyne)bis(dicobalt hexacarbonyl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.3%

: 1144513-87-0
(μ-η2-3-methoxy-3-(4'-methoxyphenyl)-1-propyne)dicobalt hexacarbonyl

: 65979-04-6
(3-(4-methoxyphenyl)-1-propyne)dicobalthexacarbonyl

: 610802-79-4,610802-80-7
(μ,η2-3,4-bis(4'-methoxyphenyl)-1,5-hexadiyne)bis(dicobalt hexacarbonyl)

Guidance literature:: With Tf₂O; Cp₂Co; In dichloromethane; (N2) Tf2O was added dropwise to soiln. Co complex in CH2Cl2 at -50°C, react. mixt. was brought to -10°C in 30 min, soln. Cp2Co in CH2Cl2 was added dropwise at -50°C, stirred for 10 min; brine was added, warmed to 0°C in 40 min, extd. with ether, washed with water, dried over Na2SO4, evapd. in vacuo, prep. TLC - mixt. diastereomers;
DOI:10.1021/om2006497