Carbonylchloro(η5-cyclopentadienyl)[(dimethylphosphino)(4-methylphenyl)keten](trimethylphosphan)wolfram

Base Information

• Chemical Name: Carbonylchloro(η5-cyclopentadienyl)[(dimethylphosphino)(4-methylphenyl)keten](trimethylphosphan)wolfram
• CAS No.: 84500-58-3
• Molecular Formula: C₂₀H₂₇ClO₂P₂W
• Molecular Weight: 580.684

Synonyms:

Chemical Property of Carbonylchloro(η5-cyclopentadienyl)[(dimethylphosphino)(4-methylphenyl)keten](trimethylphosphan)wolfram

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of Carbonylchloro(η5-cyclopentadienyl)[(dimethylphosphino)(4-methylphenyl)keten](trimethylphosphan)wolfram

There total 1 articles about Carbonylchloro(η5-cyclopentadienyl)[(dimethylphosphino)(4-methylphenyl)keten](trimethylphosphan)wolfram which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

carbonyl(η5-cyclopentadienyl)(η2-4-methylphenylketenyl)trimethylphosphinetungsten + chlorodimethylphosphine (811-62-1) → Carbonylchloro(η5-cyclopentadienyl)[(dimethylphosphino)(4-methylphenyl)keten](trimethylphosphan)wolfram (84500-58-3,89302-66-9,89708-93-0)

Guidance literature:

In dichloromethane; under Ar, dropping of chlorodimethylphosphine to the solution of η2-ketenyl complex in dichloromethane at room temp. stirred for 1 h; evapn. in vac., extn. with ether/pentane, recrystn., evapn. in vac., elem. anal.;

upstream raw materials:

chlorodimethylphosphine

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