[η3(L1)Pd(II)Cl]*CHCl3

Base Information

• Chemical Name: [η3(L1)Pd(II)Cl]*CHCl3
• CAS No.: 268735-80-4
• Molecular Formula: CHCl₃*C₂₅H₁₈Cl₂NOPPd
• Molecular Weight: 676.102
• Mol file: 268735-80-4.mol

Synonyms:

Chemical Property of [η3(L1)Pd(II)Cl]*CHCl3

Chemical Property:

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Technology Process of [η3(L1)Pd(II)Cl]*CHCl3

There total 1 articles about [η3(L1)Pd(II)Cl]*CHCl3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

PdCl2(COD) + 2-(2-Ph2PC6H4N=CH)-5-Cl-C6H3OH (249920-23-8) → [η3(L1)Pd(II)Cl]*CHCl3 (268735-80-4)

Guidance literature:

In dichloromethane; in N2 atmosphere to CH2Cl2-soln. of (C8H12)PdCl2 C25H18PN(OH)Cl added, stirred at room temp. for 30 mins, refluxed for 5 mins, cooled to room temp.; solvent removed at reduced pressure, diethyl ether added, residue extd.with CHCl3, crystals filtered, dried in vac., elem. anal.;

DOI:10.1016/S0020-1693(99)00531-9

upstream raw materials:

2-(2-Ph₂PC₆H₄N=CH)-5-Cl-C₆H₃OH

Refernces