N-phenyl carbamate de cholestanyle-3β

Base Information

• Chemical Name: N-phenyl carbamate de cholestanyle-3β
• CAS No.: 84551-46-2
• Molecular Formula: C₃₄H₅₃NO₂
• Molecular Weight: 507.8
• Mol file: 84551-46-2.mol

Synonyms:

Chemical Property of N-phenyl carbamate de cholestanyle-3β

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-phenyl carbamate de cholestanyle-3β

There total 3 articles about N-phenyl carbamate de cholestanyle-3β which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

Cholestanol (80-97-7) + phenyl isocyanate (103-71-9) → N-phenyl carbamate de cholestanyle-3β (84551-46-2,95782-88-0)

Guidance literature:

aluminium trichloride; In diethyl ether; for 1h; Ambient temperature;

Reference yield: 79.0%

3-β-cholestanol (80-97-7) + phenyl isocyanate (103-71-9) → N-phenyl carbamate de cholestanyle-3β (84551-46-2,95782-88-0)

Guidance literature:

In various solvent(s); for 15h; Ambient temperature;

Reference yield:

chloroformiate de cholestanyle-3β (36043-80-8,65928-81-6,75765-60-5) → N-phenyl carbamate de cholestanyle-3β (84551-46-2,95782-88-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 22 percent / hexamethylphosphoric acid triamide / 12 h / Irradiation

2: 79 percent / various solvent(s) / 15 h / Ambient temperature

In N,N,N,N,N,N-hexamethylphosphoric triamide;

upstream raw materials:

3-β-cholestanol

phenyl isocyanate

Cholestanol

chloroformiate de cholestanyle-3β

Downstream raw materials:

N-methyl N-phenyl carbamate de cholestanyle-3β

N-phenyl thiocarbamate de cholestanyle-3β