C₂₀H₁₄ClN₅OS

Base Information

Chemical Name:C₂₀H₁₄ClN₅OS
CAS No.:1269467-56-2
Molecular Formula:C₂₀H₁₄ClN₅OS
Molecular Weight:407.883
Hs Code.:

C<sub>20</sub>H<sub>14</sub>ClN<sub>5</sub>OS

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₁₄ClN₅OS

Chemical Property:

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Technology Process of C₂₀H₁₄ClN₅OS

There total 8 articles about C₂₀H₁₄ClN₅OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1269468-24-7
6-(4H-1,2,4-triazol-3-yl)thieno[3,2-c]quinolin-4(5H)-one

: 1269467-56-2
C₂₀H₁₄ClN₅OS

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; trichlorophosphate / acetonitrile / 100 °C

2: 1-methyl-pyrrolidin-2-one / 120 - 160 °C / Microwave irradiation

With triethylamine; trichlorophosphate; In 1-methyl-pyrrolidin-2-one; acetonitrile;
DOI:10.1016/j.bmcl.2012.02.099

Reference yield:

: 1269468-22-5
4-oxo-4,5-dihydrothieno[3.2-c]quinoline-6-carboxarnide

: 1269467-56-2
C₂₀H₁₄ClN₅OS

Guidance literature:: Multi-step reaction with 4 steps

1: 80 °C / Neat (no solvent)

2: hydrazine hydrate / acetic acid / 80 °C

3: triethylamine; trichlorophosphate / acetonitrile / 100 °C

4: 1-methyl-pyrrolidin-2-one / 120 - 160 °C / Microwave irradiation

With hydrazine hydrate; triethylamine; trichlorophosphate; In 1-methyl-pyrrolidin-2-one; acetic acid; acetonitrile;
DOI:10.1016/j.bmcl.2012.02.099

Reference yield:

: 1269468-20-3
4-oxo-4,5-dihydrothieno[3.2-c]quinoline-6-carboxylic acid

: 1269467-56-2
C₂₀H₁₄ClN₅OS

Guidance literature:: Multi-step reaction with 5 steps

1: ammonium chloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / 1-methyl-pyrrolidin-2-one / 80 °C

2: 80 °C / Neat (no solvent)

3: hydrazine hydrate / acetic acid / 80 °C

4: triethylamine; trichlorophosphate / acetonitrile / 100 °C

5: 1-methyl-pyrrolidin-2-one / 120 - 160 °C / Microwave irradiation

With ammonium chloride; benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; trichlorophosphate; In 1-methyl-pyrrolidin-2-one; acetic acid; acetonitrile;
DOI:10.1016/j.bmcl.2012.02.099