Triisopropyl-((S)-2-{(R)-5-[2-(4-methoxy-benzyloxy)-eth-(Z)-ylidene]-tetrahydro-pyran-2-yl}-6-methyl-hept-5-enyloxy)-silane

Base Information

Chemical Name:Triisopropyl-((S)-2-{(R)-5-[2-(4-methoxy-benzyloxy)-eth-(Z)-ylidene]-tetrahydro-pyran-2-yl}-6-methyl-hept-5-enyloxy)-silane
CAS No.:374901-05-0
Molecular Formula:C₃₂H₅₄O₄Si
Molecular Weight:530.864
Hs Code.:

Synonyms:

Suppliers and Price of Triisopropyl-((S)-2-{(R)-5-[2-(4-methoxy-benzyloxy)-eth-(Z)-ylidene]-tetrahydro-pyran-2-yl}-6-methyl-hept-5-enyloxy)-silane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Triisopropyl-((S)-2-{(R)-5-[2-(4-methoxy-benzyloxy)-eth-(Z)-ylidene]-tetrahydro-pyran-2-yl}-6-methyl-hept-5-enyloxy)-silane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Triisopropyl-((S)-2-{(R)-5-[2-(4-methoxy-benzyloxy)-eth-(Z)-ylidene]-tetrahydro-pyran-2-yl}-6-methyl-hept-5-enyloxy)-silane

There total 11 articles about Triisopropyl-((S)-2-{(R)-5-[2-(4-methoxy-benzyloxy)-eth-(Z)-ylidene]-tetrahydro-pyran-2-yl}-6-methyl-hept-5-enyloxy)-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 337971-14-9
(R)-(5'Z)-triisopropyl{2-[5'-[2''-(4'''-methoxybenzyloxy)ethylidene]tetrahydropyran-2'-yl]allyloxy}silane

: 374901-05-0
Triisopropyl-((S)-2-{(R)-5-[2-(4-methoxy-benzyloxy)-eth-(Z)-ylidene]-tetrahydro-pyran-2-yl}-6-methyl-hept-5-enyloxy)-silane

Guidance literature:: Multi-step reaction with 5 steps

1.1: 9-BBN / tetrahydrofuran

1.2: 21 percent / 30 percent H₂O₂; NaOH / tetrahydrofuran

2.1: 70 percent / n-Bu₃P

3.1: oxone / H₂O

4.1: n-BuLi / hexamethylphosphoric acid triamide

5.1: Na(Hg); Na₂HPO₄*12H₂O

With Oxone; disodium hydrogenphosphate; 9-borabicyclo[3.3.1]nonane dimer; n-butyllithium; sodium amalgam; tributylphosphine; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; water;
DOI:10.1246/cl.2001.898

Reference yield:

: 13154-24-0
triisopropylsilyl chloride

: 374901-05-0
Triisopropyl-((S)-2-{(R)-5-[2-(4-methoxy-benzyloxy)-eth-(Z)-ylidene]-tetrahydro-pyran-2-yl}-6-methyl-hept-5-enyloxy)-silane

Guidance literature:: Multi-step reaction with 4 steps

1: imidazole

2: oxone / H₂O

3: n-BuLi / hexamethylphosphoric acid triamide

4: Na(Hg); Na₂HPO₄*12H₂O

With 1H-imidazole; Oxone; disodium hydrogenphosphate; n-butyllithium; sodium amalgam; In N,N,N,N,N,N-hexamethylphosphoric triamide; water;
DOI:10.1246/cl.2001.898

Reference yield:

: (S)-2-{(R)-5-[2-(4-Methoxy-benzyloxy)-eth-(Z)-ylidene]-tetrahydro-pyran-2-yl}-3-phenylsulfanyl-propan-1-ol

: 374901-05-0
Triisopropyl-((S)-2-{(R)-5-[2-(4-methoxy-benzyloxy)-eth-(Z)-ylidene]-tetrahydro-pyran-2-yl}-6-methyl-hept-5-enyloxy)-silane

Guidance literature:: Multi-step reaction with 4 steps

1: imidazole

2: oxone / H₂O

3: n-BuLi / hexamethylphosphoric acid triamide

4: Na(Hg); Na₂HPO₄*12H₂O

With 1H-imidazole; Oxone; disodium hydrogenphosphate; n-butyllithium; sodium amalgam; In N,N,N,N,N,N-hexamethylphosphoric triamide; water;
DOI:10.1246/cl.2001.898