Technology Process of C19H14Cl2N6O2
There total 8 articles about C19H14Cl2N6O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
at 20 ℃;
for 2h;
Cooling with ice;
DOI:10.1002/cjoc.201090296
- Guidance literature:
-
Multi-step reaction with 6 steps
1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C
2: ammonium hydroxide / tetrahydrofuran / 20 °C / Cooling with ice
3: thionyl chloride / N,N-dimethyl-formamide / 3.25 h / 5 - 20 °C / Cooling with ice
4: potassium permanganate; potassium dihydrogenphosphate / water; acetone / 1 h / Reflux
5: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C
6: pyridine / dichloromethane / 2 h / 20 °C / Cooling with ice
With
pyridine; ammonium hydroxide; potassium permanganate; potassium dihydrogenphosphate; thionyl chloride; oxalyl dichloride; N,N-dimethyl-formamide;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1002/cjoc.201090296
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium permanganate; potassium dihydrogenphosphate / water; acetone / 1 h / Reflux
2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C
3: pyridine / dichloromethane / 2 h / 20 °C / Cooling with ice
With
pyridine; potassium permanganate; potassium dihydrogenphosphate; oxalyl dichloride; N,N-dimethyl-formamide;
In
dichloromethane; water; acetone;
DOI:10.1002/cjoc.201090296
