(1,1'-ferrocenediyl)diphenylgermane

Base Information

• Chemical Name: (1,1'-ferrocenediyl)diphenylgermane
• CAS No.: 75349-16-5
• Molecular Formula: C₂₂H₁₈FeGe
• Molecular Weight: 410.822
• Mol file: 75349-16-5.mol

Synonyms:

Chemical Property of (1,1'-ferrocenediyl)diphenylgermane

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of (1,1'-ferrocenediyl)diphenylgermane

There total 1 articles about (1,1'-ferrocenediyl)diphenylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

ferrocene (102-54-5,55404-68-7) + dichlorodiphenylgermane (1613-66-7) → (1,1'-ferrocenediyl)diphenylgermane (75349-16-5)

Guidance literature:

With (CH₃)2NCH₂CH₂N(CH₃)2; n-C₄H₉Li; In hexane; Me2NCH2CH2NMe2 and n-C4H9Li added to stirred ferrocene in n-hexane, stirred for 18 h, cooled to -78°C, Cl2GePh2 in n-hexane added, warmed to room temp., refluxed for 1 h; cooled, stirred for 30 min with water, filtered, filtrate washed with water, dried over MgSO4, filtered, evapd., ppt. filtered off, washed withcold n-hexane, dried in vac., filtrate chromd.; elem. anal.;

DOI:10.1016/S0022-328X(00)90295-X

upstream raw materials:

ferrocene

dichlorodiphenylgermane