Technology Process of C50H50N5O16PS
There total 13 articles about C50H50N5O16PS which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1H-tetrazole; dapsone;
In
pyridine;
for 0.666667h;
Yield given;
Ambient temperature;
DOI:10.1021/jo971797o
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 2.) DDS, 1H-tetrazole / 1.) pyridine, room temperature, 4 h, 2.) 3.5 h
2: 0.2N KOH / pyridine / 0.67 h / Ambient temperature
3: 1H-tetrazole, DDS / pyridine / 0.67 h / Ambient temperature
With
1H-tetrazole; potassium hydroxide; dapsone;
In
pyridine;
DOI:10.1021/jo971797o
- Guidance literature:
-
Multi-step reaction with 10 steps
3: 53 percent / XN3
4: 1.) PPh3, 2.) NH4OH / 1.) pyridine, room temperature, 3 h, 2.) H2O, 3 h
5: 89 percent / dimethylformamide / 0.02 h
6: 99 percent / pyridine / 12 h / Ambient temperature
7: 96 percent / Bu4NF*H2O, AcOH / tetrahydrofuran / 0.67 h / Ambient temperature
8: 2.) DDS, 1H-tetrazole / 1.) pyridine, room temperature, 4 h, 2.) 3.5 h
9: 0.2N KOH / pyridine / 0.67 h / Ambient temperature
10: 1H-tetrazole, DDS / pyridine / 0.67 h / Ambient temperature
With
1H-tetrazole; potassium hydroxide; ammonium hydroxide; tetrabutyl ammonium fluoride; acetic acid; triphenylphosphine; dapsone;
In
tetrahydrofuran; pyridine; N,N-dimethyl-formamide;
DOI:10.1021/jo971797o
