C₂₂H₂₆

Base Information

• Chemical Name: C₂₂H₂₆
• CAS No.: 222158-44-3
• Molecular Formula: C₂₂H₂₆
• Molecular Weight: 290.448
• Mol file: 222158-44-3.mol

Synonyms:

Chemical Property of C₂₂H₂₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₂₆

There total 12 articles about C₂₂H₂₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C22H24 (222158-89-6) → C22H26 (222158-44-3)

Guidance literature:

Multi-step reaction with 5 steps

1: CH₂Cl₂

3: 9,10-dicyanoanthracene / CD₂Cl₂ / 20 °C / Irradiation; reagent: 1,2,4,5-tetracyanobenzene, reagent absence

4: 59 percent Spectr_. / 9,10-dicyanoanthracene / CD₂Cl₂ / 3 h / 20 °C / Irradiation

5: 9,10-dicyanoanthracene / benzene-d6 / 20 °C / Irradiation

With 9,10-Dicyanoanthracene; In dichloromethane; dichloromethane-d2; benzene-d6;

DOI:10.1021/jo981775h

Reference yield:

(1S,4R,5R,6S)-5,6-Dimethyl-1,4-di-p-tolyl-2,3-diaza-bicyclo[2.2.2]oct-2-ene (222158-94-3) → C22H26 (222158-44-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 9,10-dicyanoanthracene / CD₂Cl₂ / 20 °C / Irradiation; reagent: 1,2,4,5-tetracyanobenzene, reagent absence

2: 59 percent Spectr_. / 9,10-dicyanoanthracene / CD₂Cl₂ / 3 h / 20 °C / Irradiation

3: 9,10-dicyanoanthracene / benzene-d6 / 20 °C / Irradiation

With 9,10-Dicyanoanthracene; In dichloromethane-d2; benzene-d6;

DOI:10.1021/jo981775h

Reference yield:

((1R,6S)-6-Hydroxymethyl-2,5-di-p-tolyl-cyclohexa-2,4-dienyl)-methanol (222158-87-4) → C22H26 (222158-44-3)

Guidance literature:

Multi-step reaction with 7 steps

1: pyridine

2: LiEt₃BH / tetrahydrofuran

3: CH₂Cl₂

5: 9,10-dicyanoanthracene / CD₂Cl₂ / 20 °C / Irradiation; reagent: 1,2,4,5-tetracyanobenzene, reagent absence

6: 59 percent Spectr_. / 9,10-dicyanoanthracene / CD₂Cl₂ / 3 h / 20 °C / Irradiation

7: 9,10-dicyanoanthracene / benzene-d6 / 20 °C / Irradiation

With pyridine; 9,10-Dicyanoanthracene; lithium triethylborohydride; In tetrahydrofuran; dichloromethane; dichloromethane-d2; benzene-d6;

DOI:10.1021/jo981775h

upstream raw materials:

4'-methylpropiophenone

2-bromo-4'-methylpropiophenone

C₂₂H₂₄

C₂₂H₂₆

Downstream raw materials:

C₂₂H₂₆

endo,cis-1,4-bis(4-methylphenyl)-2,3-dimethylbicyclo<2.2.0>hexane