3-phenyl-2,4,11-trimethylprodigiosene hydrochloride

Base Information

Chemical Name:3-phenyl-2,4,11-trimethylprodigiosene hydrochloride
CAS No.:105235-16-3
Molecular Formula:C₂₂H₂₁N₃*ClH
Molecular Weight:363.89
Hs Code.:

Synonyms:

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Chemical Property of 3-phenyl-2,4,11-trimethylprodigiosene hydrochloride

Chemical Property:

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Technology Process of 3-phenyl-2,4,11-trimethylprodigiosene hydrochloride

There total 9 articles about 3-phenyl-2,4,11-trimethylprodigiosene hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.6%

: 3274-55-3
2,4-dimethyl-3-phenyl-1H-pyrrole

: 105235-03-8
5-(1-methylpyrrol-2-yl)pyrrole-2-carbaldehyde

: 105235-16-3,105257-14-5
3-phenyl-2,4,11-trimethylprodigiosene hydrochloride

Guidance literature:: With L-valine hydrochloride; In ethanol; at 30 ℃; for 0.333333h;

Reference yield:

: 96-54-8
N-Methylpyrrole

: 105235-16-3,105257-14-5
3-phenyl-2,4,11-trimethylprodigiosene hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 34.4 percent / phosphorus oxychloride / diethyl ether / 2.5 h / 0 - 20 °C

2: 48.8 percent / palladium-on-charcoal / xylene / 5 h / Heating

3: 22.7 percent / benzoyl chloride / diethyl ether / 6 h / 20 °C

4: 53.6 percent / 25percent w/v HCl / ethanol / 0.33 h / 30 °C

With L-valine hydrochloride; benzoyl chloride; trichlorophosphate; palladium on activated charcoal; In diethyl ether; ethanol; xylene;

Reference yield:

: 453590-48-2
1-methyl-2-(4,5-dihydro-3H-pyrrol-2-yl)pyrrole

: 105235-16-3,105257-14-5
3-phenyl-2,4,11-trimethylprodigiosene hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 48.8 percent / palladium-on-charcoal / xylene / 5 h / Heating

2: 22.7 percent / benzoyl chloride / diethyl ether / 6 h / 20 °C

3: 53.6 percent / 25percent w/v HCl / ethanol / 0.33 h / 30 °C

With L-valine hydrochloride; benzoyl chloride; palladium on activated charcoal; In diethyl ether; ethanol; xylene;