K⁽¹⁺⁾*(OCH₂CH₂)6*[Fe((C₆H₅)4C₂₀H₈N₄)(CH₃C₃H₂N₂)2]^(1-)=[K((OCH₂CH₂)6)][Fe((C₆H₅)4C₂₀H₈N₄)(CH₃C₃H₂N₂)2]

Base Information

• Chemical Name: K⁽¹⁺⁾*(OCH₂CH₂)6*[Fe((C₆H₅)4C₂₀H₈N₄)(CH₃C₃H₂N₂)2]^(1-)=[K((OCH₂CH₂)6)][Fe((C₆H₅)4C₂₀H₈N₄)(CH₃C₃H₂N₂)2]
• CAS No.: 80925-71-9
• Molecular Formula: C₁₂H₂₄O₆*C₅₂H₃₈FeN₈*K
• Molecular Weight: 1134.19

Synonyms:

Chemical Property of K⁽¹⁺⁾*(OCH₂CH₂)6*[Fe((C₆H₅)4C₂₀H₈N₄)(CH₃C₃H₂N₂)2]^(1-)=[K((OCH₂CH₂)6)][Fe((C₆H₅)4C₂₀H₈N₄)(CH₃C₃H₂N₂)2]

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Technology Process of K⁽¹⁺⁾*(OCH₂CH₂)6*[Fe((C₆H₅)4C₂₀H₈N₄)(CH₃C₃H₂N₂)2]^(1-)=[K((OCH₂CH₂)6)][Fe((C₆H₅)4C₂₀H₈N₄)(CH₃C₃H₂N₂)2]

There total 1 articles about K⁽¹⁺⁾*(OCH₂CH₂)6*[Fe((C₆H₅)4C₂₀H₈N₄)(CH₃C₃H₂N₂)2]^(1-)=[K((OCH₂CH₂)6)][Fe((C₆H₅)4C₂₀H₈N₄)(CH₃C₃H₂N₂)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

meso-tetraphenylporphyrin iron(III) chloride (16456-81-8,170645-84-8) + 18-crown-6 ether (17455-13-9) + potassium 4-methylimidazolate → K(1+)*(OCH2CH2)6*[Fe((C6H5)4C20H8N4)(CH3C3H2N2)2](1-)=[K((OCH2CH2)6)][Fe((C6H5)4C20H8N4)(CH3C3H2N2)2] (80925-71-9)

Guidance literature:

In toluene; under Ar or He, to 1 mM soln. of Fe complex in toluene added 3.8 equiv of K(CH3C3H2N2) and 13.3 equiv of 18C6, stirred for 4 h; filtered, solid redissolved in DMA, toluene added followed by cooling to -20°C, ppt. filtered off, dried in vac.; elem. anal.;

DOI:10.1021/ja00373a042

Reference yield:

K(1+)*(OCH2CH2)6*[Fe((C6H5)4C20H8N4)(CH3C3H2N2)2](1-)=[K((OCH2CH2)6)][Fe((C6H5)4C20H8N4)(CH3C3H2N2)2] (80925-71-9) → K(1+)*(OCH2CH2)6*CH3C3H2N2(1-)=[K((OCH2CH2)6)](CH3C3H2N2) + Fe((C6H5)4C20H8N4)(CH3C3H2N2) (80925-73-1)

Guidance literature:

In toluene; dissolution in toluene; not isolated;

DOI:10.1021/ja00373a042

Reference yield:

K(1+)*(OCH2CH2)6*[Fe((C6H5)4C20H8N4)(CH3C3H2N2)2](1-)=[K((OCH2CH2)6)][Fe((C6H5)4C20H8N4)(CH3C3H2N2)2] (80925-71-9) + toluene-4-sulfonic acid (104-15-4) → Fe((C6H5)4C20H8N4)(CH3C3H2N2)*CH3C3H3N2 (80925-69-5,1008132-27-1)

Guidance literature:

In toluene; under Ar or He, solid Fe complex dissolved in toluene, p-toluenesulfonic acid added; not isolated; detected by UV;

DOI:10.1021/ja00373a042

upstream raw materials:

meso-tetraphenylporphyrin iron(III) chloride

18-crown-6 ether

Downstream raw materials:

Fe((C₆H₅)4C₂₀H₈N₄)(CH₃C₃H₂N₂)

Fe((C₆H₅)4C₂₀H₈N₄)(CH₃C₃H₂N₂)*CH₃C₃H₃N₂

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