C₂₇H₁₉F₆NS₂

Base Information

• Chemical Name: C₂₇H₁₉F₆NS₂
• CAS No.: 1364381-27-0
• Molecular Formula: C₂₇H₁₉F₆NS₂
• Molecular Weight: 535.577
• Mol file: 1364381-27-0.mol

Synonyms:

Chemical Property of C₂₇H₁₉F₆NS₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₇H₁₉F₆NS₂

There total 3 articles about C₂₇H₁₉F₆NS₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(2,3,3,4,4,5,5-heptafluorocyclopentenyl)-5-methyl-2-phenylthiazole (500004-36-4) + 2,4-dimethyl-5-phenyl-3-bromothiophene (362513-28-8) → C27H19F6NS2 (1364381-27-0)

Guidance literature:

2,4-dimethyl-5-phenyl-3-bromothiophene; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; Flow microreactor;

4-(2,3,3,4,4,5,5-heptafluorocyclopentenyl)-5-methyl-2-phenylthiazole; In tetrahydrofuran; hexane; at 0 ℃; Flow microreactor;

DOI:10.1002/cssc.201100376

Reference yield:

4-bromo-5-methyl-2-phenylthiazoline (210490-49-6) → C27H19F6NS2 (1364381-27-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 24 °C / Flow microreactor

1.2: 24 °C / Flow microreactor

2.1: n-butyllithium / tetrahydrofuran; hexane / 0 °C / Flow microreactor

2.2: 0 °C / Flow microreactor

With n-butyllithium; In tetrahydrofuran; hexane;

DOI:10.1002/cssc.201100376

Reference yield:

octaperfluorocyclopentene (559-40-0) + 4-bromo-5-methyl-2-phenylthiazoline (210490-49-6) + 2,4-dimethyl-5-phenyl-3-bromothiophene (362513-28-8) → C27H19F6NS2 (1364381-27-0)

Guidance literature:

4-bromo-5-methyl-2-phenylthiazoline; With n-butyllithium; In tetrahydrofuran; hexane; Flow microreactor;

octaperfluorocyclopentene; In tetrahydrofuran; hexane; Flow microreactor;

2,4-dimethyl-5-phenyl-3-bromothiophene; With n-butyllithium; In tetrahydrofuran; hexane; Flow microreactor;

DOI:10.1002/cssc.201100376

upstream raw materials:

octaperfluorocyclopentene

4-bromo-5-methyl-2-phenylthiazoline

2,4-dimethyl-5-phenyl-3-bromothiophene

4-(2,3,3,4,4,5,5-heptafluorocyclopentenyl)-5-methyl-2-phenylthiazole