1-trimethylstannyl-3-chloro(phenyl)borylferrocene

Base Information

Chemical Name:1-trimethylstannyl-3-chloro(phenyl)borylferrocene
CAS No.:473544-62-6
Molecular Formula:C₁₉H₂₂BClFeSn
Molecular Weight:471.205
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-trimethylstannyl-3-chloro(phenyl)borylferrocene

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Technology Process of 1-trimethylstannyl-3-chloro(phenyl)borylferrocene

There total 1 articles about 1-trimethylstannyl-3-chloro(phenyl)borylferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 70595-34-5
1,1'-bis(trimethylstannyl)ferrocene

: 873-51-8
phenylborondichloride

: 223114-56-5
1-trimethylstannyl-2-chloro(phenyl)borylferrocene

: 473544-62-6
1-trimethylstannyl-3-chloro(phenyl)borylferrocene

: 473544-63-7
1-trimethylstannyl-1'-chloro(phenyl)borylferrocene

Guidance literature:: In hexane; a soln. of C6F5BCl2 in hexane was added dropwise to a soln. of complex in hexane at -78°C, stirred at -78°C for 1 h then allowed to slowly warm to 0°C, stirred for ca. 5 days (N2); volatiles were removed under reduced pressure (1E-3 Torr), kept under dynamic vac. at ambient temp. over 1 h, isomers were detected by NMR spectra;
DOI:10.1021/om0204890