Benzenesulfonyl-9 tetradecanediol-1,10 diacetate

Base Information

Chemical Name:Benzenesulfonyl-9 tetradecanediol-1,10 diacetate
CAS No.:105866-15-7
Molecular Formula:C₂₄H₃₈O₆S
Molecular Weight:454.628
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenesulfonyl-9 tetradecanediol-1,10 diacetate

Chemical Property:

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Technology Process of Benzenesulfonyl-9 tetradecanediol-1,10 diacetate

There total 2 articles about Benzenesulfonyl-9 tetradecanediol-1,10 diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51308-99-7
9-chloro-1-nonanol

: 105866-15-7,105866-23-7
Benzenesulfonyl-9 tetradecanediol-1,10 diacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / NaI / dimethylformamide / 42 h / 65 °C

With sodium iodide; In N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(86)80010-2

Reference yield:

: 873-55-2
sodium benzenesulfonate

: 105866-15-7,105866-23-7
Benzenesulfonyl-9 tetradecanediol-1,10 diacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / NaI / dimethylformamide / 42 h / 65 °C

With sodium iodide; In N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(86)80010-2

Reference yield:

: 105866-15-7,105866-23-7
Benzenesulfonyl-9 tetradecanediol-1,10 diacetate

: 16725-53-4
(Z)-9-tetradecen-1-yl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: powdered sodium hydroxide / dioxane / 14 h / Ambient temperature; further solvents were also used

2: Adogen, sodium dithionite, NaHCO₃ / cyclohexane; H₂O / 2 h / Heating

3: pyridine / 4 h / Ambient temperature

With sodium hydroxide; sodium dithionite; triisooctyl amine; sodium hydrogencarbonate; In 1,4-dioxane; pyridine; cyclohexane; water;
DOI:10.1016/0040-4020(86)80010-2