N-Benzyltris(dimethylamino)phosphine imide

Base Information

• Chemical Name: N-Benzyltris(dimethylamino)phosphine imide
• CAS No.: 126307-69-5
• Molecular Formula: C₁₃H₂₅N₄P
• Molecular Weight: 268.342
• DSSTox Substance ID: DTXSID301151489
• Nikkaji Number: J1.246.661G
• Mol file: 126307-69-5.mol

Synonyms:DTXSID301151489;N-Benzyltris(dimethylamino)phosphine imide;N,N,N',N',N'',N''-Hexamethyl-N'''-(phenylmethyl)phosphorimidic triamide;126307-69-5

Chemical Property of N-Benzyltris(dimethylamino)phosphine imide

Chemical Property:

• XLogP3: 2.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 268.18168381
• Heavy Atom Count: 18
• Complexity: 265

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CN(C)P(=NCC1=CC=CC=C1)(N(C)C)N(C)C

Technology Process of N-Benzyltris(dimethylamino)phosphine imide

There total 3 articles about N-Benzyltris(dimethylamino)phosphine imide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

C16H34N4PSi(1+)*I(1-) → hexamethyltriamido-N-benzylimidophosphate (126307-69-5)

Guidance literature:

With ammonia; sodium;

Reference yield:

tris(dimethylamino)(trimethylsilylimino)phosphorane (53167-50-3) → hexamethyltriamido-N-benzylimidophosphate (126307-69-5)

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / 12 h / 170 °C

2: 70 percent / liquid ammonia, sodium

With ammonia; sodium; In acetonitrile;

Reference yield:

benzyl chloride (100-44-7) → hexamethyltriamido-N-benzylimidophosphate (126307-69-5)

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / 12 h / 170 °C

2: 70 percent / liquid ammonia, sodium

With ammonia; sodium; In acetonitrile;

upstream raw materials:

tris(dimethylamino)(trimethylsilylimino)phosphorane

benzyl chloride