Technology Process of C14H21NO4S
There total 18 articles about C14H21NO4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: ChiralPak-AD / tetrahydrofuran; hexane; tert-butyl methyl ether
2: tris-(dibenzylideneacetone)dipalladium(0); tributylphosphine; caesium carbonate / 1,4-dioxane / 170 °C / Microwave irradiation
3: methanol / 25 °C
4: hydrogenchloride / 1,4-dioxane / 25 °C
5: hydrogenchloride; water / methanol / 25 °C
6: boron tribromide / dichloromethane / 0 °C
With
hydrogenchloride; tris-(dibenzylideneacetone)dipalladium(0); tributylphosphine; water; boron tribromide; caesium carbonate;
In
tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; tert-butyl methyl ether;
2: Suzuki cross-coupling;
DOI:10.1016/j.bmcl.2011.02.038
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride; water / methanol / 25 °C
2: boron tribromide / dichloromethane / 0 °C
With
hydrogenchloride; water; boron tribromide;
In
methanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.02.038