(2R,3R)-3-O-(2,6-dichlorobenzyl)-1,2-O-isopropylidene-1,2,3-butanetriol

Base Information

Chemical Name:(2R,3R)-3-O-(2,6-dichlorobenzyl)-1,2-O-isopropylidene-1,2,3-butanetriol
CAS No.:104487-57-2
Molecular Formula:C₁₄H₁₈Cl₂O₃
Molecular Weight:305.201
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R)-3-O-(2,6-dichlorobenzyl)-1,2-O-isopropylidene-1,2,3-butanetriol

Chemical Property:

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Technology Process of (2R,3R)-3-O-(2,6-dichlorobenzyl)-1,2-O-isopropylidene-1,2,3-butanetriol

There total 3 articles about (2R,3R)-3-O-(2,6-dichlorobenzyl)-1,2-O-isopropylidene-1,2,3-butanetriol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15186-48-8
2,3-isopropylidene-glyceraldehyde

: 104487-57-2
(2R,3R)-3-O-(2,6-dichlorobenzyl)-1,2-O-isopropylidene-1,2,3-butanetriol

Guidance literature:: Multi-step reaction with 3 steps

1: 0.66 g / diethyl ether / 2 h / Ambient temperature

2: 63 percent

3: 1.) NaH, DMSO / 1.) THF; 2.) THF, 24 h, 25 degC

With sodium hydride; dimethyl sulfoxide; In diethyl ether;
DOI:10.1002/jlac.198719870103

Reference yield:

: 61821-85-0
(2,2-Dimethyl-[1,3]dioxolan-4-yl)-ethanol

: 104487-57-2
(2R,3R)-3-O-(2,6-dichlorobenzyl)-1,2-O-isopropylidene-1,2,3-butanetriol

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent

2: 1.) NaH, DMSO / 1.) THF; 2.) THF, 24 h, 25 degC

With sodium hydride; dimethyl sulfoxide;
DOI:10.1002/jlac.198719870103

Reference yield:

: 74183-62-3
(1RS,4'R)-1-<2',2'-Dimethyl-1',3'-dioxolan-4'-yl>aethanol

: 2014-83-7
1,3-Dichloro-2-chloromethyl-benzene

: 104487-56-1
(2R,3S)-3-O-(2,6-dichlorobenzyl)-1,2-O-isopropylidene-1,2,3-butanetriol

: 104487-57-2
(2R,3R)-3-O-(2,6-dichlorobenzyl)-1,2-O-isopropylidene-1,2,3-butanetriol

Guidance literature:: With sodium hydride; dimethyl sulfoxide; Yield given. Multistep reaction; 1.) THF; 2.) THF, 24 h, 25 degC;
DOI:10.1002/jlac.198719870103