H₃Ru₃Co(CO)10((C₆H₅)2PCH₂CH₂P(C₆H₅)2)

Base Information

• Chemical Name: H₃Ru₃Co(CO)10((C₆H₅)2PCH₂CH₂P(C₆H₅)2)
• CAS No.: 105059-22-1
• Molecular Formula: C₃₆H₂₇CoO₁₀P₂Ru₃
• Molecular Weight: 1043.76
• Mol file: 105059-22-1.mol

Synonyms:

Chemical Property of H₃Ru₃Co(CO)10((C₆H₅)2PCH₂CH₂P(C₆H₅)2)

Chemical Property:

Purity/Quality:

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Technology Process of H₃Ru₃Co(CO)10((C₆H₅)2PCH₂CH₂P(C₆H₅)2)

There total 1 articles about H₃Ru₃Co(CO)10((C₆H₅)2PCH₂CH₂P(C₆H₅)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

Ru3CoH3*12CO=Ru3CoH3(CO)12 → H3Ru3Co(CO)10((C6H5)2PCH2CH2P(C6H5)2) (105059-22-1)

Guidance literature:

With C₂H₄(P(C₆H₅)2)2; catalyst: Ph₂O^(1-) radical; In tetrahydrofuran; adding a few of Ph2O*(1-) in THF to a soln. of the complex and dppe (N2), stirring (1 h, room temp., N2); evag., chromy. (silica gel), eluting a yellow fraction with hexane, eluting H3Ru3Co(CO)10(dppe) with CH2Cl2/hexane (red band);

DOI:10.1016/S0022-328X(00)99584-6