(η4-1-phenyl-1,3,4-trimethylphospholium)(1-hydroxy-1-oxo-3,4-dimethylphospholato-(2,3,4,5,O-η))iron hydrate

Base Information

Chemical Name:(η4-1-phenyl-1,3,4-trimethylphospholium)(1-hydroxy-1-oxo-3,4-dimethylphospholato-(2,3,4,5,O-η))iron hydrate
CAS No.:78529-71-2
Molecular Formula:C₁₉H₂₄FeO₂P₂*H₂O
Molecular Weight:420.208
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (η4-1-phenyl-1,3,4-trimethylphospholium)(1-hydroxy-1-oxo-3,4-dimethylphospholato-(2,3,4,5,O-η))iron hydrate

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Technology Process of (η4-1-phenyl-1,3,4-trimethylphospholium)(1-hydroxy-1-oxo-3,4-dimethylphospholato-(2,3,4,5,O-η))iron hydrate

There total 1 articles about (η4-1-phenyl-1,3,4-trimethylphospholium)(1-hydroxy-1-oxo-3,4-dimethylphospholato-(2,3,4,5,O-η))iron hydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 67887-86-9
3,3',4,4'-tetramethyl-1,1'-diphosphaferrocene

: 591-51-5
phenyllithium

: 78529-71-2
(η4-1-phenyl-1,3,4-trimethylphospholium)(1-hydroxy-1-oxo-3,4-dimethylphospholato-(2,3,4,5,O-η))iron hydrate

Guidance literature:: With water; In tetrahydrofuran; diethyl ether; THF soln. of Fe complex was treated under Ar at -80°C with PhLi in ether; after 15 min MeI was added to the soln.; react. time 0.5 h; treating with water, extn. with EtOAc, evapn., chromy. on silica gel (EtOH); crystn. from EtOAc/pentane; elem. anal.;
DOI:10.1021/ic50224a023