1-(p-cyanophenyl)-2-ferrocenylethylene

Base Information

Chemical Name:1-(p-cyanophenyl)-2-ferrocenylethylene
CAS No.:98063-53-7
Molecular Formula:C₁₉H₁₅FeN
Molecular Weight:313.182
Hs Code.:

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Chemical Property of 1-(p-cyanophenyl)-2-ferrocenylethylene

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Technology Process of 1-(p-cyanophenyl)-2-ferrocenylethylene

There total 1 articles about 1-(p-cyanophenyl)-2-ferrocenylethylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: [1-(triphenylphosphinomethyl)ferrocenyl]iodide

: 105-07-7
4-cyanobenzaldehyde

: 123931-07-7,98063-53-7,98243-44-8
1-(p-cyanophenyl)-2-ferrocenylethylene

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; N2-atmosphere; stirring Fe-complex with 1.5 equiv. of t-BuOK for 30 min,addn. of excess of aldehyde, stirring for 24 h; solvent removal (reduced pressure), extn. into CH2Cl2, chromy. (SiO2, hexane/CH2Cl2/Me2CO=12:8:1), recrystn. (CH2Cl2/hexane); elem. anal.;
DOI:10.1016/S0022-328X(98)00569-5

Reference yield: 73.0%

: 16369-17-8,14438-11-0
2-amino-4-methylpentan-1-ol

: 123931-07-7,98063-53-7,98243-44-8
1-(p-cyanophenyl)-2-ferrocenylethylene

: 685087-91-6
1-ethenyl-(4-(4'-isobutyl-3',4'-dihydrooxazol-2'-yl)phenyl)ferrocene

Guidance literature:: zinc(II) chloride; In toluene; all manipulations under purified N2 atm.; Fe compd., org. compd. and catalytic amt. of ZnCl2 dissolved in toluene at room temp., refluxed for 8 d (monitored by TLC); filtered, solvent removed in vac., chromy. (SiO2, EtAc/hexane 1:1), solvent removed; elem. anal.;
DOI:10.1016/j.poly.2003.10.013

Reference yield: 52.0%

: 96-20-8,13054-87-0
2-aminobutanol

: 123931-07-7,98063-53-7,98243-44-8
1-(p-cyanophenyl)-2-ferrocenylethylene

: 685087-97-2
1-ethenyl-(4-(4'-ethyl-3',4'-dihydrooxazol-2'-yl)phenyl)ferrocene

Guidance literature:: zinc(II) chloride; In toluene; all manipulations under purified N2 atm.; Fe compd., org. compd. and catalytic amt. of ZnCl2 dissolved in toluene at room temp., refluxed for 8 d (monitored by TLC); filtered, solvent removed in vac., chromy. (SiO2, EtAc/hexane 1:1), solvent removed; elem. anal.;
DOI:10.1016/j.poly.2003.10.013