benzyl 2-acetamido-4,6-O-benzylidene-3-<amino>-2,3-dideoxy-α-D-glucopyranoside

Base Information

• Chemical Name: benzyl 2-acetamido-4,6-O-benzylidene-3-<amino>-2,3-dideoxy-α-D-glucopyranoside
• CAS No.: 108432-64-0
• Molecular Formula: C₂₅H₃₀N₂O₇
• Molecular Weight: 470.522
• Mol file: 108432-64-0.mol

Synonyms:

Chemical Property of benzyl 2-acetamido-4,6-O-benzylidene-3-<amino>-2,3-dideoxy-α-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzyl 2-acetamido-4,6-O-benzylidene-3-<amino>-2,3-dideoxy-α-D-glucopyranoside

There total 6 articles about benzyl 2-acetamido-4,6-O-benzylidene-3-<amino>-2,3-dideoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

benzyl 2-acetamido-4,6-O-benzylidene-2,3-dideoxy-3-<amino>-α-D-glucopyranoside (105528-61-8,105528-62-9,108508-12-9,108508-14-1) → benzyl 2-acetamido-4,6-O-benzylidene-3-<amino>-2,3-dideoxy-α-D-glucopyranoside (108432-64-0,108432-66-2)

Guidance literature:

With potassium hydroxide; Ambient temperature; 1.) ethanol, 20 h, 2.) water, Amberlite IRC-50(H⁺);

DOI:10.1016/S0040-4020(01)87561-X

Reference yield: 77.0%

benzyl 2-acetamido-4,6-O-benzylidene-2,3-dideoxy-3-<amino>-α-D-glucopyranoside (105528-61-8,105528-62-9,108508-12-9,108508-14-1) → benzyl 2-acetamido-4,6-O-benzylidene-3-<amino>-2,3-dideoxy-α-D-glucopyranoside (108432-64-0,108432-66-2)

Guidance literature:

With potassium hydroxide; Ambient temperature; 1.) ethanol, 20 deg C, 2.) water, Amberlite IRC-50(H⁺);

DOI:10.1016/S0040-4020(01)87561-X

Reference yield:

benzyl 2-acetamido-3-amino-4,6-O-benzylidene-2,3-dideoxy-α-D-glucopyranoside (53910-43-3,61330-53-8,107983-28-8) → benzyl 2-acetamido-4,6-O-benzylidene-3-<amino>-2,3-dideoxy-α-D-glucopyranoside (108432-64-0,108432-66-2)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / acetonitrile / 20 h / Heating

2: 79 percent / 1.) 1percent KOH / Ambient temperature; 1.) ethanol, 20 h, 2.) water, Amberlite IRC-50(H⁺)

With pyridine; potassium hydroxide; In acetonitrile;

DOI:10.1016/S0040-4020(01)87561-X

upstream raw materials:

benzyl 2-acetamido-4,6-O-benzylidene-2,3-dideoxy-3-<amino>-α-D-glucopyranoside

methyl 2-acetamido-3-amino-4,6-O-bezylidene-2,3-dideoxy-α-D-glucopyranoside

benzyl 2-acetamido-3-amino-4,6-O-benzylidene-2,3-dideoxy-α-D-glucopyranoside

benzyl 2-acetamido-4,6-O-benzylidene-2,3-dideoxy-3-<amino>-α-D-glucopyranoside

Downstream raw materials:

N-(benzyl-2-acetamido-4,6-O-benzylidene-2,3-dideoxy-α-D-glucopyranosid-3-yl)-D-alanyl-D-glutamine methyl ester

N-(benzyl-2-acetamido-4,6-O-benzylidene-2,3-dideoxy-α-D-glucopyranosid-3-yl)-D-alanyl-D-isoglutamine methyl ester

N-(benzyl 2-acetamido-4,6-O-benzylidene-2,3-dideoxy-α-D-glucopyranosid-3-yl)-D-alanyl-L-alanyl-D-isoglutamine methyl ester

N-(benzyl 2-acetamido-4,6-O-benzylidene-2,3-dideoxy-α-D-glucopyranosid-3-yl)-D-alanyl-L-alanyl-D-glutamine methyl ester