C₃₃H₅₅BrOSi₂

Base Information

Chemical Name:C₃₃H₅₅BrOSi₂
CAS No.:1542211-35-7
Molecular Formula:C₃₃H₅₅BrOSi₂
Molecular Weight:603.874
Hs Code.:

C<sub>33</sub>H<sub>55</sub>BrOSi<sub>2</sub>

Synonyms:

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Chemical Property of C₃₃H₅₅BrOSi₂

Chemical Property:

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Technology Process of C₃₃H₅₅BrOSi₂

There total 4 articles about C₃₃H₅₅BrOSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1542211-33-5
5-(hexadecyloxy)-1,3-diiodo-2-methylbenzene

: 1542211-35-7
C₃₃H₅₅BrOSi₂

Guidance literature:: Multi-step reaction with 2 steps

1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diethylamine / 35 °C

2: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 20 h / Reflux; Schlenk technique; Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; copper(l) iodide; diethylamine; dibenzoyl peroxide; In tetrachloromethane; 1: |Sonogashira Cross-Coupling;
DOI:10.1021/ja412606t

Reference yield:

: 24540-55-4
3,5-diiodo-p-cresol

: 1542211-35-7
C₃₃H₅₅BrOSi₂

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / ethanol / 18 h / 95 °C / Inert atmosphere; Schlenk technique

2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diethylamine / 35 °C

3: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 20 h / Reflux; Schlenk technique; Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; copper(l) iodide; diethylamine; sodium hydroxide; dibenzoyl peroxide; In tetrachloromethane; ethanol; 2: |Sonogashira Cross-Coupling;
DOI:10.1021/ja412606t

Reference yield:

: 112-82-3
hexadecanyl bromide

: 1542211-35-7
C₃₃H₅₅BrOSi₂

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / ethanol / 18 h / 95 °C / Inert atmosphere; Schlenk technique

2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diethylamine / 35 °C

3: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 20 h / Reflux; Schlenk technique; Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; copper(l) iodide; diethylamine; sodium hydroxide; dibenzoyl peroxide; In tetrachloromethane; ethanol; 2: |Sonogashira Cross-Coupling;
DOI:10.1021/ja412606t