(((C₂H₅)P(C₆H₅)2)Ni(C₃H₄OO))4

Base Information

Chemical Name:(((C₂H₅)P(C₆H₅)2)Ni(C₃H₄OO))4
CAS No.:838848-33-2
Molecular Formula:C₆₈H₇₆Ni₄O₈P₄
Molecular Weight:1380
Hs Code.:

(((C<sub>2</sub>H<sub>5</sub>)P(C<sub>6</sub>H<sub>5</sub>)2)Ni(C<sub>3</sub>H<sub>4</sub>OO))4

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Chemical Property of (((C₂H₅)P(C₆H₅)2)Ni(C₃H₄OO))4

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Technology Process of (((C₂H₅)P(C₆H₅)2)Ni(C₃H₄OO))4

There total 2 articles about (((C₂H₅)P(C₆H₅)2)Ni(C₃H₄OO))4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 779355-57-6
(pyridine)₂Ni{CH₂CH₂C(=O)O}

: 607-01-2
ethyl-diphenyl-phosphane

: 838848-33-2
(((C₂H₅)P(C₆H₅)2)Ni(C₃H₄OO))4

Guidance literature:: In N,N-dimethyl-formamide; byproducts: pyridine; Ar atm., the mixt. of complex and phosphine in DMF was stirred for 30 min at room temp.; filtered, the solvent was slowly distilled at room temp. under recued pressure, the redisue was treated with ether with rapid stirring, solid was filtered and dried in a vac.;
DOI:10.1021/om040111x

Reference yield: 53.0%

: 1295-35-8
bis(1,5-cyclooctadiene)nickel ⁽⁰⁾

: 57-57-8
β-Propiolactone

: 607-01-2
ethyl-diphenyl-phosphane

: 838848-33-2
(((C₂H₅)P(C₆H₅)2)Ni(C₃H₄OO))4

Guidance literature:: In tetrahydrofuran; Ar atm.; to a stirred mixt. of complex and phosphine in THF was added succinic anhydride at 0°C, the soln. was allowed to warm to room temp., stirred for 1 h, heated to 40°C for 30 min; the solvent was removed in vac., ether was added, solids were removed byfiltration, crystals were obtained from the soln. at 5°C for a f ew days, decanted, crystals were dried in a vac.; elem. anal.;
DOI:10.1021/om040111x