diferrocenyl(trityloxy)cyclopropenylium tetrafluoroborate

Base Information

Chemical Name:diferrocenyl(trityloxy)cyclopropenylium tetrafluoroborate
CAS No.:862772-15-4
Molecular Formula:BF₄*C₄₂H₃₃Fe₂O
Molecular Weight:752.222
Hs Code.:

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Chemical Property of diferrocenyl(trityloxy)cyclopropenylium tetrafluoroborate

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Technology Process of diferrocenyl(trityloxy)cyclopropenylium tetrafluoroborate

There total 1 articles about diferrocenyl(trityloxy)cyclopropenylium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 56551-49-6
2,3-diferrocenylcyclopropenone

: 341-02-6
trityl tetrafluoroborate

: 862772-15-4
diferrocenyl(trityloxy)cyclopropenylium tetrafluoroborate

Guidance literature:: In dichloromethane; soln. of triphenylcarbenium tetrafluoroborate in CH2Cl2 was added in dryN2 atm. with stirring to soln. of diferrocenylcyclopropenone in CH2Cl2; mixt. stirred for 1 h at 20°C; dry Et2O added; ppt. filtered off; washed (dry ether); dried (vac.); elem. anal.;
DOI:10.1016/j.jorganchem.2005.04.014

Reference yield: 68.0%

: 862772-15-4
diferrocenyl(trityloxy)cyclopropenylium tetrafluoroborate

: 865-47-4
potassium tert-butylate

: triphenylmethyl 2,3-diferrocenylacrylate

Guidance literature:: In benzene; byproducts: (CH3)2CCH2; stirring mixt. of the tetrafluoroborate salt and t-BuOK in dry benzene was boiled under reflux in inert dry atm. for 3 h; solvent evapd.; residue purified by chromy. on alumina (hexane-ether, 4:1); elem. anal.;
DOI:10.1016/j.jorganchem.2005.04.014