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C58H92IN15O14

Base Information
  • Chemical Name:C58H92IN15O14
  • CAS No.:1316857-51-8
  • Molecular Formula:C58H92IN15O14
  • Molecular Weight:1350.37
  • Hs Code.:
C<sub>58</sub>H<sub>92</sub>IN<sub>15</sub>O<sub>14</sub>

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Chemical Property of C58H92IN15O14
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Technology Process of C58H92IN15O14

There total 10 articles about C58H92IN15O14 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With copper(l) iodide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 25 ℃; for 15h;
DOI:10.1039/c1ob05606a
Guidance literature:
Multi-step reaction with 6 steps
1: hydrogenchloride; methanol / 4 h / 50 °C
2: sodium hydroxide / water; dimethyl sulfoxide / 18 h / 25 °C
3: zinc trifluoromethanesulfonate; triethylamine / dichloromethane / 20 h / 25 °C
4: copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 15 h / 25 °C
5: methanol; potassium carbonate / 1.5 h / 25 °C
6: copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 15 h / 25 °C
With hydrogenchloride; methanol; copper(l) iodide; zinc trifluoromethanesulfonate; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; 4: Huisgen-Sharpless 1,3-dipolar cycloaddition / 6: Huisgen-Sharpless 1,3-dipolar cycloaddition;
DOI:10.1039/c1ob05606a
Guidance literature:
Multi-step reaction with 5 steps
1: sodium hydroxide / water; dimethyl sulfoxide / 18 h / 25 °C
2: zinc trifluoromethanesulfonate; triethylamine / dichloromethane / 20 h / 25 °C
3: copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 15 h / 25 °C
4: methanol; potassium carbonate / 1.5 h / 25 °C
5: copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 15 h / 25 °C
With methanol; copper(l) iodide; zinc trifluoromethanesulfonate; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; 3: Huisgen-Sharpless 1,3-dipolar cycloaddition / 5: Huisgen-Sharpless 1,3-dipolar cycloaddition;
DOI:10.1039/c1ob05606a
upstream raw materials:

C14H26N6O4

C14H17IO4

C12H17IO4

C21H23IO4

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