Technology Process of C58H92IN15O14
There total 10 articles about C58H92IN15O14 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
copper(l) iodide; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran;
at 25 ℃;
for 15h;
DOI:10.1039/c1ob05606a
- Guidance literature:
-
Multi-step reaction with 6 steps
1: hydrogenchloride; methanol / 4 h / 50 °C
2: sodium hydroxide / water; dimethyl sulfoxide / 18 h / 25 °C
3: zinc trifluoromethanesulfonate; triethylamine / dichloromethane / 20 h / 25 °C
4: copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 15 h / 25 °C
5: methanol; potassium carbonate / 1.5 h / 25 °C
6: copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 15 h / 25 °C
With
hydrogenchloride; methanol; copper(l) iodide; zinc trifluoromethanesulfonate; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide;
4: Huisgen-Sharpless 1,3-dipolar cycloaddition / 6: Huisgen-Sharpless 1,3-dipolar cycloaddition;
DOI:10.1039/c1ob05606a
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydroxide / water; dimethyl sulfoxide / 18 h / 25 °C
2: zinc trifluoromethanesulfonate; triethylamine / dichloromethane / 20 h / 25 °C
3: copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 15 h / 25 °C
4: methanol; potassium carbonate / 1.5 h / 25 °C
5: copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 15 h / 25 °C
With
methanol; copper(l) iodide; zinc trifluoromethanesulfonate; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide;
3: Huisgen-Sharpless 1,3-dipolar cycloaddition / 5: Huisgen-Sharpless 1,3-dipolar cycloaddition;
DOI:10.1039/c1ob05606a