C₂₈H₃₀O₆

Base Information

Chemical Name:C₂₈H₃₀O₆
CAS No.:1395786-44-3
Molecular Formula:C₂₈H₃₀O₆
Molecular Weight:462.543
Hs Code.:

C<sub>28</sub>H<sub>30</sub>O<sub>6</sub>

Synonyms:

Suppliers and Price of C₂₈H₃₀O₆

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₈H₃₀O₆

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₈H₃₀O₆

There total 7 articles about C₂₈H₃₀O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1415692-77-1
C₃₆H₃₈O₁₀

: 1395786-44-3
C₂₈H₃₀O₆

Guidance literature:: With methanol; potassium carbonate; at 20 ℃; for 1.5h;
DOI:10.1021/jm300884k

Reference yield:

: 1005142-57-3
[4-(acetoxymethyl)-2-bromo-5-chlorophenyl]methyl acetate

: 1395786-44-3
C₂₈H₃₀O₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium hydroxide; water / tetrahydrofuran; ethanol / 3 h / 80 °C

2.1: pyridinium p-toluenesulfonate / tetrahydrofuran / 2 h / 0 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.42 h / -78 °C / Inert atmosphere

3.2: 0.08 h

4.1: toluene-4-sulfonic acid / tetrahydrofuran; methanol / 15 h / 20 °C

5.1: chloro-trimethyl-silane / dimethyl sulfoxide / 4 h / 20 °C

5.2: 1 h / 0 - 20 °C

6.1: tetrabutylammomium bromide; bis(cyclopentadienyl)titanium dichloride; sodium carbonate / water; N,N-dimethyl-formamide / 15 h / 85 °C

7.1: bis(dibenzylideneacetone)-palladium⁽⁰⁾; monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; potassium fluoride / tetrahydrofuran / 0.5 h / 100 °C / Microwave irradiation

8.1: potassium carbonate; methanol / 1.5 h / 20 °C

With methanol; bis(cyclopentadienyl)titanium dichloride; potassium fluoride; n-butyllithium; chloro-trimethyl-silane; monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; tetrabutylammomium bromide; water; pyridinium p-toluenesulfonate; sodium carbonate; potassium carbonate; toluene-4-sulfonic acid; potassium hydroxide; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; methanol; ethanol; hexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm300884k

Reference yield:

: 85072-44-2
1-bromo-4-chloro-2,5-dimethylbenzene

: 1395786-44-3
C₂₈H₃₀O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / ethyl acetate / 0.33 h / Reflux

2.1: N,N-dimethyl-formamide / 3 h / 80 °C

3.1: potassium hydroxide; water / tetrahydrofuran; ethanol / 3 h / 80 °C

4.1: pyridinium p-toluenesulfonate / tetrahydrofuran / 2 h / 0 °C

5.1: n-butyllithium / tetrahydrofuran; hexane / 0.42 h / -78 °C / Inert atmosphere

5.2: 0.08 h

6.1: toluene-4-sulfonic acid / tetrahydrofuran; methanol / 15 h / 20 °C

7.1: chloro-trimethyl-silane / dimethyl sulfoxide / 4 h / 20 °C

7.2: 1 h / 0 - 20 °C

8.1: tetrabutylammomium bromide; bis(cyclopentadienyl)titanium dichloride; sodium carbonate / water; N,N-dimethyl-formamide / 15 h / 85 °C

9.1: bis(dibenzylideneacetone)-palladium⁽⁰⁾; monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; potassium fluoride / tetrahydrofuran / 0.5 h / 100 °C / Microwave irradiation

10.1: potassium carbonate; methanol / 1.5 h / 20 °C

With methanol; bis(cyclopentadienyl)titanium dichloride; potassium fluoride; N-Bromosuccinimide; n-butyllithium; chloro-trimethyl-silane; monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; 2,2'-azobis(isobutyronitrile); tetrabutylammomium bromide; water; pyridinium p-toluenesulfonate; sodium carbonate; potassium carbonate; toluene-4-sulfonic acid; potassium hydroxide; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; methanol; ethanol; hexane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm300884k