MoI(CO)2((C₆H₅)2PCH₂)2(S₂P(OC₂H₅)2)

Base Information

• Chemical Name: MoI(CO)2((C₆H₅)2PCH₂)2(S₂P(OC₂H₅)2)
• CAS No.: 404579-79-9
• Molecular Formula: C₃₂H₃₄IMoO₄P₃S₂
• Molecular Weight: 862.517
• Mol file: 404579-79-9.mol

Synonyms:

Chemical Property of MoI(CO)2((C₆H₅)2PCH₂)2(S₂P(OC₂H₅)2)

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of MoI(CO)2((C₆H₅)2PCH₂)2(S₂P(OC₂H₅)2)

There total 1 articles about MoI(CO)2((C₆H₅)2PCH₂)2(S₂P(OC₂H₅)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

ammonium O,O-diethyldithiophosphate (1068-22-0) + MoI2(CO)3(MeCN)2 (102349-56-4) + 1,2-bis-(diphenylphosphino)ethane (1663-45-2) → MoI(CO)2((C6H5)2PCH2)2(S2P(OC2H5)2) (404579-79-9)

Guidance literature:

In dichloromethane; MoI2(CO)3(NCMe)2 dissolved in CH2Cl2; NH4(S2P(OEt)2) added with stirring; after 30 min mixt. filtered; Ph2PCH2CH2PPh2 added to filtrate; soln. stirred for 30 min; hexane added; mixt. kept at 0.°C for 3 ds; elem. anal.;

DOI:10.1016/S0020-1693(01)00699-5

upstream raw materials:

ammonium O,O-diethyldithiophosphate

MoI₂(CO)3(MeCN)2

1,2-bis-(diphenylphosphino)ethane