2,7-bis(3-isopropoxyphenyl)-9-isopropylacridine

Base Information

• Chemical Name: 2,7-bis(3-isopropoxyphenyl)-9-isopropylacridine
• CAS No.: 1352136-00-5
• Molecular Formula: C₃₄H₃₅NO₂
• Molecular Weight: 489.657
• Mol file: 1352136-00-5.mol

Synonyms:

Chemical Property of 2,7-bis(3-isopropoxyphenyl)-9-isopropylacridine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,7-bis(3-isopropoxyphenyl)-9-isopropylacridine

There total 4 articles about 2,7-bis(3-isopropoxyphenyl)-9-isopropylacridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C34H37NO2 → 2,7-bis(3-isopropoxyphenyl)-9-isopropylacridine (1352136-00-5)

Guidance literature:

With potassium hydroxide; potassium hexacyanoferrate(III); In dichloromethane; water; at 20 ℃; for 20h;

DOI:10.1039/c1cc16582h

Reference yield:

2,7-bis(3-isopropoxyphenyl)acridine (1352136-08-3) → 2,7-bis(3-isopropoxyphenyl)-9-isopropylacridine (1352136-00-5)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 20 h / 70 °C / Inert atmosphere

2: potassium hydroxide; potassium hexacyanoferrate(III) / dichloromethane; water / 20 h / 20 °C

With potassium hydroxide; potassium hexacyanoferrate(III); In dichloromethane; water; toluene;

DOI:10.1039/c1cc16582h

Reference yield:

2,7-dibromoacridine (1211-37-6) → 2,7-bis(3-isopropoxyphenyl)-9-isopropylacridine (1352136-00-5)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; water / Reflux

2: toluene / 20 h / 70 °C / Inert atmosphere

3: potassium hydroxide; potassium hexacyanoferrate(III) / dichloromethane; water / 20 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; potassium hydroxide; potassium hexacyanoferrate(III); In 1,2-dimethoxyethane; dichloromethane; water; toluene;

DOI:10.1039/c1cc16582h

upstream raw materials:

2,7-bis(3-isopropoxyphenyl)acridine

2,7-dibromoacridine

3-isopropyloxyphenylboronic acid