[((CH₃)5C₅)Ru(NCCH₃)2(P(C₆H₅)2NHC₆H₅)]⁽¹⁺⁾*PF₆^(1-)=[((CH₃)5C₅)Ru(NCCH₃)2(P(C₆H₅)2NHC₆H₅)]PF₆

Base Information

• Chemical Name: [((CH₃)5C₅)Ru(NCCH₃)2(P(C₆H₅)2NHC₆H₅)]⁽¹⁺⁾*PF₆^(1-)=[((CH₃)5C₅)Ru(NCCH₃)2(P(C₆H₅)2NHC₆H₅)]PF₆
• CAS No.: 886210-49-7
• Molecular Formula: C₃₂H₃₇N₃PRu*F₆P
• Molecular Weight: 740.674

Synonyms:

Chemical Property of [((CH₃)5C₅)Ru(NCCH₃)2(P(C₆H₅)2NHC₆H₅)]⁽¹⁺⁾*PF₆^(1-)=[((CH₃)5C₅)Ru(NCCH₃)2(P(C₆H₅)2NHC₆H₅)]PF₆

Chemical Property:

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MSDS Files:

Useful:

Technology Process of [((CH₃)5C₅)Ru(NCCH₃)2(P(C₆H₅)2NHC₆H₅)]⁽¹⁺⁾*PF₆^(1-)=[((CH₃)5C₅)Ru(NCCH₃)2(P(C₆H₅)2NHC₆H₅)]PF₆

There total 1 articles about [((CH₃)5C₅)Ru(NCCH₃)2(P(C₆H₅)2NHC₆H₅)]⁽¹⁺⁾*PF₆^(1-)=[((CH₃)5C₅)Ru(NCCH₃)2(P(C₆H₅)2NHC₆H₅)]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

tris(acetonitrile)pentamethylcyclopentadienylruthenium(II) hexafluorophosphate + (diphenylphosphino)phenylamine (6230-65-5) → [((CH3)5C5)Ru(NCCH3)2(P(C6H5)2NHC6H5)](1+)*PF6(1-)=[((CH3)5C5)Ru(NCCH3)2(P(C6H5)2NHC6H5)]PF6 (886210-49-7)

Guidance literature:

In dichloromethane; under N2 or Ar, Schlenk setup; stoich. mixt. stirred at room temp. for 1h; evapd., washed (Et2O, petroleum ether), dried (vac.); elem. anal.;

DOI:10.1002/ejic.200500034

Reference yield: 56.0%

[((CH3)5C5)Ru(NCCH3)2(P(C6H5)2NHC6H5)](1+)*PF6(1-)=[((CH3)5C5)Ru(NCCH3)2(P(C6H5)2NHC6H5)]PF6 (886210-49-7) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) → [((CH3)5C5)Ru(CH3CN)(η2-(CH3OOCCHCH2)(P(C6H5)2NHC6H5)]PF6 (886210-59-9)

Guidance literature:

In dichloromethane; under N2 or Ar, Schlenk setup; ligand (1 mmol) added to metal compd. (0.5 mmol), mixt. stirred 30 min at room temp.; filtered (Celite), layered (petroleum ether), crystd., washed (petroleumether), dried (vac.); elem. anal.;

DOI:10.1002/ejic.200500034

Reference yield: 54.0%

[((CH3)5C5)Ru(NCCH3)2(P(C6H5)2NHC6H5)](1+)*PF6(1-)=[((CH3)5C5)Ru(NCCH3)2(P(C6H5)2NHC6H5)]PF6 (886210-49-7) + acetylene (74-86-2,25067-58-7) → [((CH3)5C5)Ru(η4-C4H5)(P(C6H5)2N(C6H5)-κ1N)]PF6

Guidance literature:

In dichloromethane; under N2 or Ar, Schlenk setup; acetylene bubbled through solution of metal compd. (0.5 mmol), mixt. stirred at room temp. for 1 h under acetylene, filtered, evapd.; washed (Et2O, petroleum ether), dried (vac.); recrystd. (acetone, petroleum ether), elem. anal.;

DOI:10.1002/ejic.200500034

upstream raw materials:

(diphenylphosphino)phenylamine

Downstream raw materials:

[((CH3)5C5)Ru(CH3CN)(η2-(CH3OOCCHCH2)(P(C6H5)2NHC6H5)]PF6

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