C₅H₃N(C₅H₃NCH₃)C₅H₃NC₆H₂(CH₃)3

Base Information

Chemical Name:C₅H₃N(C₅H₃NCH₃)C₅H₃NC₆H₂(CH₃)3
CAS No.:1375186-69-8
Molecular Formula:C₂₅H₂₃N₃
Molecular Weight:365.478
Hs Code.:

C<sub>5</sub>H<sub>3</sub>N(C<sub>5</sub>H<sub>3</sub>NCH<sub>3</sub>)C<sub>5</sub>H<sub>3</sub>NC<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3

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Suppliers and Price of C₅H₃N(C₅H₃NCH₃)C₅H₃NC₆H₂(CH₃)3

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅H₃N(C₅H₃NCH₃)C₅H₃NC₆H₂(CH₃)3

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Technology Process of C₅H₃N(C₅H₃NCH₃)C₅H₃NC₆H₂(CH₃)3

There total 3 articles about C₅H₃N(C₅H₃NCH₃)C₅H₃NC₆H₂(CH₃)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 626-05-1
2,6-Dibromopyridine

: 1375186-69-8
C₅H₃N(C₅H₃NCH₃)C₅H₃NC₆H₂(CH₃)3

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; copper dichloride / diethyl ether / -80 °C

2.1: n-butyllithium; tributyltin chloride / tetrahydrofuran / -78 °C

2.2: Reflux

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; Na₃PO₄*12H₂O / 1,2-dimethoxyethane; water / Reflux

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; Na₃PO₄*12H₂O; tributyltin chloride; copper dichloride; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; water; 1.1: Ullmann reaction / 2.2: Stille coupling / 3.1: Suzuki-Miyaura coupling;
DOI:10.1021/om300279t

Reference yield:

: 49669-22-9
6,6'-Dibromo-2,2'-bipyridine

: 1375186-69-8
C₅H₃N(C₅H₃NCH₃)C₅H₃NC₆H₂(CH₃)3

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium; tributyltin chloride / tetrahydrofuran / -78 °C

1.2: Reflux

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; Na₃PO₄*12H₂O / 1,2-dimethoxyethane; water / Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; Na₃PO₄*12H₂O; tributyltin chloride; In tetrahydrofuran; 1,2-dimethoxyethane; water; 1.2: Stille coupling / 2.1: Suzuki-Miyaura coupling;
DOI:10.1021/om300279t

Reference yield:

: 1375186-78-9
C₁₆H₁₂BrN₃

: 5980-97-2
mesitylboronic acid

: 1375186-69-8
C₅H₃N(C₅H₃NCH₃)C₅H₃NC₆H₂(CH₃)3

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; Na₃PO₄*12H₂O; In 1,2-dimethoxyethane; water; Reflux;
DOI:10.1021/om300279t