C₃₁H₃₀BNS

Base Information

• Chemical Name: C₃₁H₃₀BNS
• CAS No.: 1423446-98-3
• Molecular Formula: C₃₁H₃₀BNS
• Molecular Weight: 459.463
• Mol file: 1423446-98-3.mol

Synonyms:

Chemical Property of C₃₁H₃₀BNS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₁H₃₀BNS

There total 4 articles about C₃₁H₃₀BNS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(2-bromophenyl)-1H-benzo[d]thiazole (22901-00-4) → C31H30BNS (1423446-98-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere; Schlenk technique

1.2: -78 - 20 °C / Inert atmosphere; Schlenk technique

2.1: toluene / Inert atmosphere; Schlenk technique; UV-irradiation

With n-butyllithium; In tetrahydrofuran; toluene;

DOI:10.1021/ja400917r

Reference yield:

2-chlorobenzo[d][1,3]thiazole (615-20-3) → C31H30BNS (1423446-98-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; water / Inert atmosphere; Schlenk technique

2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere; Schlenk technique

2.2: -78 - 20 °C / Inert atmosphere; Schlenk technique

3.1: toluene / Inert atmosphere; Schlenk technique; UV-irradiation

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; potassium carbonate; In tetrahydrofuran; water; toluene;

DOI:10.1021/ja400917r

Reference yield:

(2-bromophenyl)boronic acid (244205-40-1) → C31H30BNS (1423446-98-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; water / Inert atmosphere; Schlenk technique

2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere; Schlenk technique

2.2: -78 - 20 °C / Inert atmosphere; Schlenk technique

3.1: toluene / Inert atmosphere; Schlenk technique; UV-irradiation

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; potassium carbonate; In tetrahydrofuran; water; toluene;

DOI:10.1021/ja400917r

upstream raw materials:

2-(2-bromophenyl)-1H-benzo[d]thiazole

2-chlorobenzo[d][1,3]thiazole

(2-bromophenyl)boronic acid

2-(2-(dimesitylboryl)phenyl)benzothiazole