Ac-Lys-Asp-Ser-Phe-Val-Gly--Leu-Met-NH2

Base Information

Chemical Name:Ac-Lys-Asp-Ser-Phe-Val-Gly--Leu-Met-NH2
CAS No.:143293-19-0
Molecular Formula:C₄₄H₇₀N₁₀O₁₂S
Molecular Weight:963.166
Hs Code.:

Ac-Lys-Asp-Ser-Phe-Val-Gly-<R-γ-Lac>-Leu-Met-NH2

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Chemical Property of Ac-Lys-Asp-Ser-Phe-Val-Gly--Leu-Met-NH2

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Technology Process of Ac-Lys-Asp-Ser-Phe-Val-Gly--Leu-Met-NH2

There total 4 articles about Ac-Lys-Asp-Ser-Phe-Val-Gly--Leu-Met-NH2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124202-00-2
(R)-2-<3-<(tert-butoxycarbonyl)amino>-2-oxo-1-pyrrolidinyl>-(S)-4-methylpentanoic acid methyl ester

: 143293-19-0
Ac-Lys-Asp-Ser-Phe-Val-Gly--Leu-Met-NH2

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / 2 M aq. NaOH / methanol / 18 h / 0 °C

2: 57 percent / DCC / dimethylformamide / 3 h / 20 °C

With sodium hydroxide; dicyclohexyl-carbodiimide; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00100a027

Reference yield:

: 82611-48-1
(2S)-2-<(3R)-3-<(tert-butoxycarbonyl)amino>-2-oxopyrrolidin-1-yl>-4-methylpentanoic acid

: 143293-19-0
Ac-Lys-Asp-Ser-Phe-Val-Gly--Leu-Met-NH2

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / DCC / dimethylformamide / 3 h / 20 °C

With dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1021/jm00100a027

Reference yield:

: 82611-46-9
N-(tert-butoxycarbonyl)-D-methionyl-L-leucine methyl ester

: 143293-19-0
Ac-Lys-Asp-Ser-Phe-Val-Gly--Leu-Met-NH2

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) CH₃I, 2.) NaH / 1.) 5 d, 2.) DMF, -40 - 3 deg C, 45 min

2: 94 percent / 2 M aq. NaOH / methanol / 18 h / 0 °C

3: 57 percent / DCC / dimethylformamide / 3 h / 20 °C

With sodium hydroxide; sodium hydride; dicyclohexyl-carbodiimide; methyl iodide; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00100a027