Technology Process of C33H34FN3O5
There total 5 articles about C33H34FN3O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: KOH / ethanol; H2O / 2.5 h / 80 °C
2: triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 1 h
With
potassium hydroxide; di-isopropyl azodicarboxylate; triphenylphosphine;
In
tetrahydrofuran; ethanol; water;
2: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2007.03.027
- Guidance literature:
-
Multi-step reaction with 5 steps
1: iron; NH4Cl / tetrahydrofuran; methanol; H2O / 3 h / 100 °C
2: LiAlH4 / tetrahydrofuran / 7 h / 20 °C
3: AcONa; AcOH / tetrahydrofuran / 1.5 h / 20 °C
4: KOH / ethanol; H2O / 2.5 h / 80 °C
5: triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 1 h
With
potassium hydroxide; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; sodium acetate; iron; ammonium chloride; acetic acid; triphenylphosphine;
In
tetrahydrofuran; methanol; ethanol; water;
5: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2007.03.027
- Guidance literature:
-
Multi-step reaction with 4 steps
1: LiAlH4 / tetrahydrofuran / 7 h / 20 °C
2: AcONa; AcOH / tetrahydrofuran / 1.5 h / 20 °C
3: KOH / ethanol; H2O / 2.5 h / 80 °C
4: triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 1 h
With
potassium hydroxide; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; sodium acetate; acetic acid; triphenylphosphine;
In
tetrahydrofuran; ethanol; water;
4: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2007.03.027
