zinc(II) complex of 1-methyl-2-[2-(5,10,15,20-tetraphenylporphyrin-2-yl)vinyl]pyridinium chloride

Base Information

• Chemical Name: zinc(II) complex of 1-methyl-2-[2-(5,10,15,20-tetraphenylporphyrin-2-yl)vinyl]pyridinium chloride
• CAS No.: 930775-02-3
• Molecular Formula: C₅₂H₃₆N₅Zn*Cl
• Molecular Weight: 831.734
• Mol file: 930775-02-3.mol

Synonyms:

Chemical Property of zinc(II) complex of 1-methyl-2-[2-(5,10,15,20-tetraphenylporphyrin-2-yl)vinyl]pyridinium chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of zinc(II) complex of 1-methyl-2-[2-(5,10,15,20-tetraphenylporphyrin-2-yl)vinyl]pyridinium chloride

There total 2 articles about zinc(II) complex of 1-methyl-2-[2-(5,10,15,20-tetraphenylporphyrin-2-yl)vinyl]pyridinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

2-formyl-5,10,15,20-tetraphenylporphyrinato zinc(II) (110350-65-7) + N-methyl-2-methylpyridinium iodide (872-73-1) → zinc(II) complex of 1-methyl-2-[2-(5,10,15,20-tetraphenylporphyrin-2-yl)vinyl]pyridinium chloride (930775-02-3) + 2-Formyl-21,23-dihydro-5,10,15,20-tetraphenylporphyrin (71159-98-3)

Guidance literature:

2-formyl-5,10,15,20-tetraphenylporphyrinato zinc(II); N-methyl-2-methylpyridinium iodide; With potassium carbonate; In tetrahydrofuran; methanol; at 30 ℃; for 1h; Inert atmosphere;

With sodium chloride; In water;

DOI:10.1142/S1088424611004373

Reference yield:

2-Formyl-21,23-dihydro-5,10,15,20-tetraphenylporphyrin (71159-98-3) → zinc(II) complex of 1-methyl-2-[2-(5,10,15,20-tetraphenylporphyrin-2-yl)vinyl]pyridinium chloride (930775-02-3)

Guidance literature:

Multi-step reaction with 2 steps

1: zinc diacetate

2: potassium carbonate / tetrahydrofuran; methanol / 1 h / 30 °C / Inert atmosphere

With zinc diacetate; potassium carbonate; In tetrahydrofuran; methanol;

DOI:10.1142/S1088424611004373

upstream raw materials:

2-formyl-5,10,15,20-tetraphenylporphyrinato zinc(II)

N-methyl-2-methylpyridinium iodide

2-Formyl-21,23-dihydro-5,10,15,20-tetraphenylporphyrin