thallium(I) oximino(2,6-dichlorophenyl)acetonitrile

Base Information

• Chemical Name: thallium(I) oximino(2,6-dichlorophenyl)acetonitrile
• CAS No.: 1032478-00-4
• Molecular Formula: C₈H₃Cl₂N₂O*Tl
• Molecular Weight: 418.414
• Mol file: 1032478-00-4.mol

Synonyms:

Chemical Property of thallium(I) oximino(2,6-dichlorophenyl)acetonitrile

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of thallium(I) oximino(2,6-dichlorophenyl)acetonitrile

There total 1 articles about thallium(I) oximino(2,6-dichlorophenyl)acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

thallium(I) carbonate + sodium salt oximino(2,6-dichlorophenyl)acetonitrile (1032477-94-3) → thallium(I) oximino(2,6-dichlorophenyl)acetonitrile (1032478-00-4)

Guidance literature:

In water; Tl2CO3 in H2O mixed with sodium salt of ligand in H2O (Tl:L=1:2), heatedto boil for 5 min, filtered into H2O at 95°C; cooled, crystd. for several d, filtered, washed (cold H2O), dried (H2SO4), elem. anal.;

DOI:10.1016/j.ica.2007.10.019

upstream raw materials:

sodium salt oximino(2,6-dichlorophenyl)acetonitrile