Cp*Zr(OC₆H-2,3,5,6-Ph₄)Cl₂

Base Information

• Chemical Name: Cp*Zr(OC₆H-2,3,5,6-Ph₄)Cl₂
• CAS No.: 1075166-13-0
• Molecular Formula: C₄₀H₃₆Cl₂OZr
• Molecular Weight: 694.855

Synonyms:

Chemical Property of Cp*Zr(OC₆H-2,3,5,6-Ph₄)Cl₂

Chemical Property:

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Technology Process of Cp*Zr(OC₆H-2,3,5,6-Ph₄)Cl₂

There total 1 articles about Cp*Zr(OC₆H-2,3,5,6-Ph₄)Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

pentamethylcyclopentadienylzirconium(IV) trichloride + Li(OC6H4-2,3,5,6-Ph4)*Et2O → Cp*Zr(OC6H-2,3,5,6-Ph4)Cl2 (1075166-13-0)

Guidance literature:

In benzene; byproducts: LiCl; under inert atm. Li(OC6H-2,3,5,6-Ph4)*Et2O was added to suspn. Cp*TiCl3 in benzene and stirred at room temp. overnight; soln. was filtered through Celite, solvent was removed in vacuo; elem. anal.;

DOI:10.1021/om8004993

Reference yield: 74.0%

methyllithium lithium bromide + Cp*Zr(OC6H-2,3,5,6-Ph4)Cl2 (1075166-13-0) → Cp*Zr(OC6H-2,3,5,6-Ph4)Me2 (1075165-99-9)

Guidance literature:

In diethyl ether; under N2 atm. to soln. Zr complex in Et2O at 0°C MeLi*LiBr was added and stirred at 0°C for 3 h; solvent was removed in vacuo and replaced with benzene, filtered throughCelite and evapd.;

DOI:10.1021/om8004993

Reference yield: 55.0%

Cp*Zr(OC6H-2,3,5,6-Ph4)Cl2 (1075166-13-0) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → Cp*Zr(OC6H-2,3,5,6-Ph4)Cl2*C6H6

Guidance literature:

In hexane; benzene;

DOI:10.1021/om8004993

Downstream raw materials:

Cp*Zr(OC₆H-2,3,5,6-Ph₄)Me₂

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