C₂₄H₂₇NO₃

Base Information

• Chemical Name: C₂₄H₂₇NO₃
• CAS No.: 1104730-05-3
• Molecular Formula: C₂₄H₂₇NO₃
• Molecular Weight: 377.483
• Mol file: 1104730-05-3.mol

Synonyms:

Chemical Property of C₂₄H₂₇NO₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₂₇NO₃

There total 2 articles about C₂₄H₂₇NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

vinyl benzoate (769-78-8,24991-32-0) + (+/-)-2-(1,8-diethyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-1-yl)ethanol (200880-25-7) → C24H27NO3 (1104730-05-3) + (1S)-(1,8-diethyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-1-yl)-1-ethanol (200880-29-1) + (1R)-(1,8-diethyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-1-yl)-1-ethanol (200880-27-9)

Guidance literature:

With Lipase A₁₂ derived from Apergillus niger; In di-isopropyl ether; at 35 ℃; for 240h; optical yield given as %ee; Resolution of racemate; Inert atmosphere; Enzymatic reaction;

DOI:10.3987/COM-08-S(N)118

Reference yield:

vinyl benzoate (769-78-8,24991-32-0) + (+/-)-2-(1,8-diethyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-1-yl)ethanol (200880-25-7) → C24H27NO3 (1104730-05-3) + C24H27NO3 + (1S)-(1,8-diethyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-1-yl)-1-ethanol (200880-29-1) + (1R)-(1,8-diethyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-1-yl)-1-ethanol (200880-27-9)

Guidance literature:

With Lipase R derived from Penicillium roqueforti; In di-isopropyl ether; at 35 ℃; for 96h; optical yield given as %ee; Resolution of racemate; Inert atmosphere; Enzymatic reaction;

DOI:10.3987/COM-08-S(N)118

upstream raw materials:

vinyl benzoate

(+/-)-2-(1,8-diethyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-1-yl)ethanol