C₄₆H₆₇N₃O₇Si₂

Base Information

Chemical Name:C₄₆H₆₇N₃O₇Si₂
CAS No.:1426656-53-2
Molecular Formula:C₄₆H₆₇N₃O₇Si₂
Molecular Weight:830.225
Hs Code.:

C<sub>46</sub>H<sub>67</sub>N<sub>3</sub>O<sub>7</sub>Si<sub>2</sub>

Synonyms:

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Chemical Property of C₄₆H₆₇N₃O₇Si₂

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Technology Process of C₄₆H₆₇N₃O₇Si₂

There total 8 articles about C₄₆H₆₇N₃O₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1426656-41-8
C₁₉H₃₂N₂O₃Si

: C₂₇H₃₆ClNO₄Si

: 1426656-53-2
C₄₆H₆₇N₃O₇Si₂

Guidance literature:: With silver cyanide; In toluene; at 0 - 80 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c3cc00178d

Reference yield:

: 159718-22-6
(2R,3R)-(+)-2-azido-3-isopropyl-3-hydroxypropionic acid

: 1426656-53-2
C₄₆H₆₇N₃O₇Si₂

Guidance literature:: Multi-step reaction with 5 steps

1: 2,6-dimethylpyridine / dichloromethane / 4 h / 0 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / methanol / 14 h / 20 °C / Inert atmosphere

3: sodium hydrogencarbonate / tetrahydrofuran; water / 16 h / 0 - 20 °C / Inert atmosphere

4: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0 °C / Inert atmosphere

5: silver cyanide / toluene / 2 h / 0 - 80 °C / Inert atmosphere

With 2,6-dimethylpyridine; silver cyanide; oxalyl dichloride; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; dichloromethane; water; toluene;
DOI:10.1039/c3cc00178d

Reference yield:

: 159990-09-7
(2R,3R)-(+)-ethyl 2-azido-3-isopropyl-3-hydroxypropionate

: 1426656-53-2
C₄₆H₆₇N₃O₇Si₂

Guidance literature:: Multi-step reaction with 6 steps

1: lithium hydroxide; water / methanol; tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

2: 2,6-dimethylpyridine / dichloromethane / 4 h / 0 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / methanol / 14 h / 20 °C / Inert atmosphere

4: sodium hydrogencarbonate / tetrahydrofuran; water / 16 h / 0 - 20 °C / Inert atmosphere

5: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0 °C / Inert atmosphere

6: silver cyanide / toluene / 2 h / 0 - 80 °C / Inert atmosphere

With 2,6-dimethylpyridine; silver cyanide; oxalyl dichloride; palladium 10% on activated carbon; water; hydrogen; sodium hydrogencarbonate; N,N-dimethyl-formamide; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; toluene;
DOI:10.1039/c3cc00178d