N-(4-(dodecyloxy)phenyl)-N,N',N',N'',N''-pentamethylguanidinium ((4-(dodecyloxy)phenyl)sulfonyl)((trifluoromethyl)sulfonyl)azanide

Base Information

Chemical Name:N-(4-(dodecyloxy)phenyl)-N,N',N',N'',N''-pentamethylguanidinium ((4-(dodecyloxy)phenyl)sulfonyl)((trifluoromethyl)sulfonyl)azanide
CAS No.:1452854-89-5
Molecular Formula:C₁₉H₂₉F₃NO₅S₂*C₂₄H₄₄N₃O
Molecular Weight:863.203
Hs Code.:

Synonyms:

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Chemical Property of N-(4-(dodecyloxy)phenyl)-N,N',N',N'',N''-pentamethylguanidinium ((4-(dodecyloxy)phenyl)sulfonyl)((trifluoromethyl)sulfonyl)azanide

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Technology Process of N-(4-(dodecyloxy)phenyl)-N,N',N',N'',N''-pentamethylguanidinium ((4-(dodecyloxy)phenyl)sulfonyl)((trifluoromethyl)sulfonyl)azanide

There total 4 articles about N-(4-(dodecyloxy)phenyl)-N,N',N',N'',N''-pentamethylguanidinium ((4-(dodecyloxy)phenyl)sulfonyl)((trifluoromethyl)sulfonyl)azanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1240016-79-8
N-(4-(dodecyloxy)phenyl)-N',N',N'',N''-tetramethylguanidinium chloride

: 1452854-89-5
N-(4-(dodecyloxy)phenyl)-N,N',N',N'',N''-pentamethylguanidinium ((4-(dodecyloxy)phenyl)sulfonyl)((trifluoromethyl)sulfonyl)azanide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 12 h / 50 °C / Inert atmosphere

2: silver nitrate / methanol / 12 h / 20 °C / Inert atmosphere; Darkness

3: acetonitrile / 0.08 h / Inert atmosphere; Reflux

With potassium carbonate; silver nitrate; In methanol; acetonitrile;
DOI:10.3762/bjoc.9.121

Reference yield:

: 1380349-61-0
4-(dodecyloxy)phenylpentamethylguanidinium iodide

: 1452854-89-5
N-(4-(dodecyloxy)phenyl)-N,N',N',N'',N''-pentamethylguanidinium ((4-(dodecyloxy)phenyl)sulfonyl)((trifluoromethyl)sulfonyl)azanide

Guidance literature:: Multi-step reaction with 2 steps

1: silver nitrate / methanol / 12 h / 20 °C / Inert atmosphere; Darkness

2: acetonitrile / 0.08 h / Inert atmosphere; Reflux

With silver nitrate; In methanol; acetonitrile;
DOI:10.3762/bjoc.9.121

Reference yield:

: 58076-34-9
4-(dodecyloxy)benzene-1-sulfonyl chloride

: 1452854-89-5
N-(4-(dodecyloxy)phenyl)-N,N',N',N'',N''-pentamethylguanidinium ((4-(dodecyloxy)phenyl)sulfonyl)((trifluoromethyl)sulfonyl)azanide

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 12 h / 40 °C / Inert atmosphere

1.2: 0.08 h / 65 °C / Inert atmosphere

2.1: acetonitrile / 0.08 h / Inert atmosphere; Reflux

With triethylamine; In dichloromethane; acetonitrile;
DOI:10.3762/bjoc.9.121