Technology Process of C24H21NO5
There total 8 articles about C24H21NO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
air;
In
methanol;
at 37 ℃;
for 195h;
aq. phosphate buffer;
DOI:10.1002/cmdc.201000537
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sodium hydride / dimethyl sulfoxide / 8 °C
2: potassium tert-butylate / tetrahydrofuran / Reflux
3: acetic acid / Reflux
4: potassium hydroxide / ethylene glycol / 1 h / 185 °C
5: copper(l) iodide; L-proline / N,N-dimethyl-formamide / 72 h / 140 °C
6: boron tribromide / dichloromethane / 0 - 20 °C
7: air / methanol / 195 h / 37 °C / aq. phosphate buffer
With
copper(l) iodide; potassium tert-butylate; boron tribromide; sodium hydride; acetic acid; L-proline; potassium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; ethylene glycol; dimethyl sulfoxide; N,N-dimethyl-formamide;
3: Fischer-Fink synthesis / 5: Ullmann reaction;
DOI:10.1002/cmdc.201000537
- Guidance literature:
-
Multi-step reaction with 2 steps
1: boron tribromide / dichloromethane / 0 - 20 °C
2: air / methanol / 195 h / 37 °C / aq. phosphate buffer
With
boron tribromide;
In
methanol; dichloromethane;
DOI:10.1002/cmdc.201000537