C₅₀H₇₉NO₁₂Si₂

Base Information

Chemical Name:C₅₀H₇₉NO₁₂Si₂
CAS No.:1402588-86-6
Molecular Formula:C₅₀H₇₉NO₁₂Si₂
Molecular Weight:942.348
Hs Code.:

C<sub>50</sub>H<sub>79</sub>NO<sub>12</sub>Si<sub>2</sub>

Synonyms:

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Chemical Property of C₅₀H₇₉NO₁₂Si₂

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Technology Process of C₅₀H₇₉NO₁₂Si₂

There total 27 articles about C₅₀H₇₉NO₁₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1402588-85-5
C₅₈H₈₇NO₁₃Si₂

: 1402588-86-6
C₅₀H₇₉NO₁₂Si₂

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; Inert atmosphere;
DOI:10.1021/ja3057612

Reference yield:

: 864514-42-1
Acetic acid (4R,6R)-4-(tert-butyl-dimethyl-silanyloxy)-6-(2-hydroxy-butyl)-5,5-dimethyl-tetrahydro-pyran-2-yl ester

: 1402588-86-6
C₅₀H₇₉NO₁₂Si₂

Guidance literature:: Multi-step reaction with 13 steps

1.1: zinc(II) iodide / acetonitrile / 0.67 h / 0 °C / Inert atmosphere

2.1: Dess-Martin periodane / 3 h / 0 °C / Inert atmosphere

3.1: phenylborondichloride; N-ethyl-N,N-diisopropylamine / dichloromethane; methanol / 3.5 h / -78 °C / Inert atmosphere

4.1: benzo[1,3,2]dioxaborole / tetrahydrofuran / 20 h / -78 - 0 °C / Inert atmosphere

5.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere

6.1: water; ethanol / 1.33 h / Reflux

7.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1 h / 20 °C / Inert atmosphere

8.1: palladium 10% on activated carbon; hydrogen / ethanol / 24 h / Inert atmosphere

9.1: N-ethyl-N,N-diisopropylamine / toluene / 0.5 h / Inert atmosphere

10.1: dichloromethane / 1.5 h / 20 °C / Inert atmosphere

11.1: N-ethyl-N,N-diisopropylamine / toluene / 1.33 h / 40 °C

11.2: 6 h / 20 °C / Inert atmosphere

12.1: N-ethyl-N,N-diisopropylamine / toluene / 4 h / 0 °C / Inert atmosphere

13.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / Inert atmosphere

With 2,6-dimethylpyridine; palladium 10% on activated carbon; phenylborondichloride; hydrogen; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; zinc(II) iodide; benzo[1,3,2]dioxaborole; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; acetonitrile;
DOI:10.1021/ja3057612

Reference yield:

: C₁₈H₃₃NO₃Si

: 1402588-86-6
C₅₀H₇₉NO₁₂Si₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: phenylborondichloride; N-ethyl-N,N-diisopropylamine / dichloromethane; methanol / 3.5 h / -78 °C / Inert atmosphere

2.1: benzo[1,3,2]dioxaborole / tetrahydrofuran / 20 h / -78 - 0 °C / Inert atmosphere

3.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere

4.1: water; ethanol / 1.33 h / Reflux

5.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1 h / 20 °C / Inert atmosphere

6.1: palladium 10% on activated carbon; hydrogen / ethanol / 24 h / Inert atmosphere

7.1: N-ethyl-N,N-diisopropylamine / toluene / 0.5 h / Inert atmosphere

8.1: dichloromethane / 1.5 h / 20 °C / Inert atmosphere

9.1: N-ethyl-N,N-diisopropylamine / toluene / 1.33 h / 40 °C

9.2: 6 h / 20 °C / Inert atmosphere

10.1: N-ethyl-N,N-diisopropylamine / toluene / 4 h / 0 °C / Inert atmosphere

11.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / Inert atmosphere

With 2,6-dimethylpyridine; palladium 10% on activated carbon; phenylborondichloride; hydrogen; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; benzo[1,3,2]dioxaborole; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene;
DOI:10.1021/ja3057612