η2-N,O-[2-(CH2N(CH2)4NMe)-6-PhC6H3O]AlMe2

Base Information

Chemical Name:η2-N,O-[2-(CH2N(CH2)4NMe)-6-PhC6H3O]AlMe2
CAS No.:1223583-24-1
Molecular Formula:C₂₀H₂₇AlN₂O
Molecular Weight:338.429
Hs Code.:

Synonyms:

Suppliers and Price of η2-N,O-[2-(CH2N(CH2)4NMe)-6-PhC6H3O]AlMe2

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of η2-N,O-[2-(CH2N(CH2)4NMe)-6-PhC6H3O]AlMe2

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of η2-N,O-[2-(CH2N(CH2)4NMe)-6-PhC6H3O]AlMe2

There total 1 articles about η2-N,O-[2-(CH2N(CH2)4NMe)-6-PhC6H3O]AlMe2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1223583-14-9
2-(CH₂N(CH₂)4NMe)-6-PhC₆H₃OH

: 75-24-1
trimethylaluminum

: 1223583-24-1
η2-N,O-[2-(CH2N(CH2)4NMe)-6-PhC6H3O]AlMe2

Guidance literature:: In dichloromethane; byproducts: CH4; N2; precooled (-35°C) soln. of ligand added to precooled (-40°C) soln. of AlMe (1:1 molar ratio), mixt. warmed to room temp. with stirring for 2 h; evapd., recrystd. (pentane/Et2O=10/1, -40°C), elem. anal.;
DOI:10.1002/ejic.200900703

Reference yield: 95.0%

: 1223583-24-1
η2-N,O-[2-(CH2N(CH2)4NMe)-6-PhC6H3O]AlMe2

: 1109-15-5
tris(pentafluorophenyl)borate

: 1223583-36-5
[η3-N,O,N-[2-(CH2N(CH2)4NMe)-6-PhC6H3O]AlMe][MeB(C6F5)3]

Guidance literature:: In dichloromethane; N2; B(C6F5)3 added with stirring to soln. of Al compd. (1:1 molar ratio)at room temp., mixt. stirred at room temp. for 30 min; evapd., trirurated (pentane), filtered off, dried (vac.), elem. anal.;
DOI:10.1002/ejic.200900703