acetyl-DL-2,4,5-trifluorophenylalanine

Base Information

Chemical Name:acetyl-DL-2,4,5-trifluorophenylalanine
CAS No.:324028-04-8
Molecular Formula:C₁₁H₁₀F₃NO₃
Molecular Weight:261.201
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of acetyl-DL-2,4,5-trifluorophenylalanine

Chemical Property:

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Technology Process of acetyl-DL-2,4,5-trifluorophenylalanine

There total 3 articles about acetyl-DL-2,4,5-trifluorophenylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 324027-98-7
2-acetylamino-2-(2,4,5-trifluoro-benzyl)-malonic acid

: 324028-04-8
acetyl-DL-2,4,5-trifluorophenylalanine

Guidance literature:: In xylene; at 139 ℃; for 2h;
DOI:10.1246/bcsj.73.2531

Reference yield:

: 157911-56-3
2,4,5-trifluorobenzyl bromide

: 324028-04-8
acetyl-DL-2,4,5-trifluorophenylalanine

Guidance literature:: Multi-step reaction with 3 steps

1: Na; C₂H₅OH / 2 h / Heating

2: NaOH; HCl / methanol / 3 h / 40 °C

3: xylene / 2 h / 139 °C

With hydrogenchloride; sodium hydroxide; ethanol; sodium; In methanol; xylene;
DOI:10.1246/bcsj.73.2531

Reference yield:

: 324027-92-1
diethyl 2-acetamido-2-(2,4,5-trifluorobenzyl)malonate

: 324028-04-8
acetyl-DL-2,4,5-trifluorophenylalanine

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH; HCl / methanol / 3 h / 40 °C

2: xylene / 2 h / 139 °C

With hydrogenchloride; sodium hydroxide; In methanol; xylene;
DOI:10.1246/bcsj.73.2531